N-(2-溴苯基)甲烷磺酰胺合成路线 （共 4 条）
反应条件
pyridine 3 h; Ambient temperature;
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Iwashita, Shigeki; Nagano, Tatsuo; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1988 , vol. 36, # 4 p. 1305 - 1308
反应条件
T=20°C; Acylation; condensation; 0.0166667 h;
参考文献
Cai, Lisheng; Han, Ying; Ren, Sumei; Huang, Liangfu
Tetrahedron, 2000 , vol. 56, # 42 p. 8253 - 8262
反应条件
1: Pd(PPh3)2Cl2, Et3N / dimethylformamide / 24 h / 120 °C
2: 15 percent / CuI, Et3N / dimethylformamide / 3 h / 80 °C
View Scheme
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Iwashita, Shigeki; Nagano, Tatsuo; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1988 , vol. 36, # 4 p. 1305 - 1308
反应条件
caesium carbonate in acetonitrile
T=20°C; 24 h;
参考文献
CEPHALON, INC.; CURRY, Matthew A.; DORSEY, Bruce D.; DUGAN, Benjamin J.; GINGRICH, Diane E.; MESAROS, Eugen F.; MILKIEWICZ, Karen L.
Patent: WO2010/141796 A2, 2010 ;
Location in patent: Page/Page column 276 ;
