1165952-91-9合成路线 （共 295 条）
反应条件
bis(1,5-cyclooctadiene)nickel (0); diethylaluminium chloride; triphenylphosphine in toluene T=50°C; 48 h; other ligands, var. P/Ni and Al/Ni ratios, var. reaction times; Product distribution;
参考文献
Cros, Philippe; Triantaphylides, Christian; Buono, Gerard
Journal of Organic Chemistry, 1988 , vol. 53, # 1 p. 185 - 187
反应条件
zeolite H-BEA in toluene T=111°C; Title compound not separated from byproducts;
参考文献
Jimenez, Oriol; Mueller, Thomas E.; Schwieger, Wilhelm; Lercher, Johannes A.
Journal of Catalysis, 2006 , vol. 239, # 1 p. 42 - 50
反应条件
1: 75 percent / 168 h / Ambient temperature 2: SOCl2 / 2 h / Heating 3: 85 percent / CH2Cl2; ethyl acetate / 2 h View Scheme
参考文献
Pitha, Josef; Szabo, Lajos; Szurmai, Zoltan; Buchowiecki, Wieslaw; Kusiak, John W.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 1 p. 96 - 100
反应条件
dihydrogen peroxide; copper(l) chloride in 1,2-dichloro-ethane; acetonitrile T=20°C; Diels-Alder reaction;
参考文献
Kalita, Biswajit; Nicholas, Kenneth M.
Tetrahedron Letters, 2005 , vol. 46, # 9 p. 1451 - 1453
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; caesium acetate; copper(l) chloride; 2,2,2-trimethylacetic acid in ethanol; acetone T=20°C; Diels-Alder Cycloaddition; 48 h;
参考文献
Yang, Wei; Sun, Jiaqiong; Xu, Xianxiu; Zhang, Qian; Liu, Qun
Chemical Communications, 2014 , vol. 50, # 34 p. 4420 - 4422
反应条件
bismuth trifluoromethanesulphonate; [Cu(I)(CH3CN)4]PF6; 1,2-bis-(diphenylphosphino)ethane in 1,4-dioxane T=50°C; 3 h;
参考文献
Journal of the American Chemical Society, , vol. 128, # 5 p. 1611 - 1614
反应条件
[(9,9-Me2-4,5-(PPh2)2-xanthene]Pd(η3-allyl)Cl in tetrahydrofuran T=50°C; 24 h;
参考文献
Journal of the American Chemical Society, , vol. 128, # 6 p. 1828 - 1839
反应条件
silver trifluoromethanesulfonate in toluene T=90°C; 0.5 h; Inert atmosphereDarknessMicrowave irradiationair stream cooling;
参考文献
Giner, Xavier; Najera, Carmen; Kovacs, Gabor; Lledos, Agusti; Ujaque, Gregori
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 18 p. 3451 - 3466
反应条件
in ethanol; water RuCl3*nH2O was dissolved in 90 percent EtOH followed by dropwise addn. 1,3-cyclohexadiene, heated to reflux (85°C) for 4 h; ppt. was filtered off, washed with EtOH and dried in vacuo;
参考文献
Inorganic Chemistry, , vol. 50, # 19 p. 9714 - 9727
反应条件
in ethanol treating soln. of RuCl3 (0.0065 mol) in 90percent alc. with 1.3-cyclohexadiene (0.0065 mol), stirring mixt. for 3 h at 45°C; pptn., filtering after 12 h, washing with alc. and ether, drying in vac.; elem. anal.;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, p. 1922 - 1926
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 2071 - 2076
