1165952-91-9合成路线 （共 295 条）
参考文献
Carman, Raymond M.; Smith, Stephanie S.
Australian Journal of Chemistry, 1981 , vol. 34, # 6 p. 1285 - 1294
反应条件
bis(1,5-cyclooctadiene)nickel (0); trifluoroacetic acid in toluene T=20°C; 14 h;
参考文献
Yale University
Patent: US6384282 B2, 2002 ;
Location in patent: Page column 23-24 ;
反应条件
1: Cu2Cl2, nPrCO2Na, PdCl2, HC(OMe)3 / 2280 Torr 2: (i) (hydrogenation), (ii) (hydrolysis) View Scheme
参考文献
Stille,J.K.; Divakaruni,R.
Journal of Organic Chemistry, 1979 , vol. 44, # 2 p. 3474 - 3482
反应条件
hydrogen bromide; acetic acid
参考文献
Hofmann; Damm
Mitt. Kohlenforschungsinst. Breslau, vol. 2, p. 127
Chem. Zentralbl., 1926 , vol. 97, # I p. 2342
参考文献
Cornubert; Rio; Senechal
Bulletin de la Societe Chimique de France, 1955 , p. 46,50
Full Text Show Details
Sakashita
Nippon Kagaku Zasshi, 1959 , vol. 80, p. 972,973
Chem.Abstr., 1960 , p. 2008
参考文献
Harland, Philip A.; Hodge, Philip
Synthesis, 1983 , # 5 p. 419 - 421
反应条件
1: 1.) stannic chloride, 2.) triethylamine / 1.) methylene chloride, -20 deg C, 10 min, 2.) methylene chloride, room temperature, 10 min 2: 58 percent / W-2 Raney nickel / ethanol / 1.5 h / Heating View Scheme
参考文献
Ishibashi, Hiroyuki; Okada, Motofumi; Nakatani, Hiroshi; Ikeda, Masazumi; Tamura, Yasumitsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1763 - 1768
反应条件
in tetrahydrofuran T=-75°C; hetero-Diels-Alder reaction; 22 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 45, # 1 p. 149 - 154
反应条件
hydrogen; dodecacarbonyltetrarhodium(0); [Re(CO)5]H in hexane T=34.84°C; P=30003 Torr; Autocalve;
参考文献
AGENCY FOR SCIENCE, TECHNOLOGY AND RESEARCH; LI, Chuanzhao; JACOB, Chacko; KANICHI, Sa-Ei; GARLAND, Marc
Patent: WO2011/28180 A1, 2011 ;
Location in patent: Page/Page column 16 ;
反应条件
triphenyl phosphite; rhodium(I)(acetylacetonate)(phenylphosphite)2; hydrogen T=80°C; P=7600 Torr; 3 h; Title compound not separated from byproducts;
参考文献
Journal of Organometallic Chemistry, , vol. 479, # 1-2 p. 213 - 216
