1165952-91-9合成路线 （共 295 条）
反应条件
selenium; caesium carbonate in acetonitrile T=50°C;
参考文献
Abelman, Matthew M.
Tetrahedron Letters, 1991 , vol. 32, # 50 p. 7389 - 7392
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; 1,3-bis-(diphenylphosphino)propane; sodium carbonate in toluene T=140°C; 20 h; Inert atmosphere; regioselective reaction;
参考文献
Banerjee, Debasis; Junge, Kathrin; Beller, Matthias
Angewandte Chemie - International Edition, 2014 , vol. 53, # 6 p. 1630 - 1635
Angew. Chem., 2014 , vol. 126, # 6 p. 1656 - 1661,6
反应条件
in tetrachloromethane; ethanol T=-20°C; 480 h;
参考文献
Liebigs Annalen der Chemie, , # 2 p. 202 - 209
反应条件
1: o-Hydroxymethyl-benzoldiazonium With Merrifield resin modified with piperazine in tetrahydrofuran T=0 - 25°C; Solid phase reaction; 2: cyclohexa-1,3-diene With palladium diacetate; trifluoroacetic acid in methanol T=40°C; cleavage-cross-coupling; 2 h;
参考文献
Braese, Stefan; Schroen, Maarten
Angewandte Chemie - International Edition, 1999 , vol. 38, # 8 p. 1071 - 1073
参考文献
Zhao, Xiaodong Edward
Patent: US2003/4242 A1, 2003 ;
反应条件
1.1: tetrahydrofuran / 18 h / 60 °C 2.1: palladium on activated charcoal; hydrogen / ethyl acetate / 2 h 3.1: sodium hydroxide; water / methanol / 8 h / 60 °C 3.2: pH 1 4.1: acetic anhydride / 1.5 h / 100 °C View Scheme
参考文献
SUNSHINE LAKE PHARMA CO., LTD.; ZHANG, Yingjun; ZHANG, Jiancun; XIE, Hongming; REN, Qingyun; TAN, Yumei; LUO, Huichao
Patent: WO2014/19344 A1, 2014 ;
反应条件
Hydrieren an Palladium in Aceton, Erwaermen mit aethanol. Kalilauge und mit Acetylchlorid;
参考文献
Diels; Alder
Justus Liebigs Annalen der Chemie, 1931 , vol. 490, p. 257,263
反应条件
hydrogenchloride T=-8 - -5°C;
参考文献
Berlande
Bulletin de la Societe Chimique de France, 1942 , vol. <5> 9, p. 644,651, 652
反应条件
in pentane T=-80°C; 2 h; Product distribution;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 177, # 11 p. 2639 - 2650
参考文献
Courtot; Pierron
Bulletin de la Societe Chimique de France, 1929 , vol. <4>45, p. 290
