1165952-91-9合成路线 （共 295 条）
反应条件
hydrogen; silica gel; Pt/Al2O3 T=170°C; 48 h; examination of hydrogenation var. time and reag;;
参考文献
Bulletin de la Societe Chimique de France, , vol. 1, # 7-8 p. 258 - 264
反应条件
sodium amide in ammonia T=-50°C; 3 h; var. alkali amides; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 48, # 23 p. 4266 - 4271
反应条件
in acetone T=20°C; diastereoselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 48, # 32 p. 5958 - 5961
反应条件
in tetrahydrofuran (Ar); soln. of cyclohexadiene was added to Mo complex and mixt. was heated at 50°C for 1 h; red-orange needles pptd. and were sepd.; identified by IR and UV;
参考文献
Journal of Organometallic Chemistry, , vol. 282, p. 357 - 362
反应条件
in benzene-d6 under N2 for 7-10 min (molar ratio metal hydride:diene = ca. 2:1);; detected by CIDNP studies;;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 4 p. 312 - 314
反应条件
in benzene-d6 under N2 for 7-10 min (molar ratio metal hydride:diene = ca. 2:1);; detected by CIDNP studies;;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 4 p. 312 - 314
反应条件
bis(acetylacetonate)nickel(II); triethylaluminum in toluene T=25°C; other solvent; KineticsRate constant;
参考文献
Chemische Berichte, , vol. 122, p. 1919 - 1924
反应条件
in diphenylether T=260°C; various temp., solvents; ΔG(excit.), ΔH(excit.), ΔS(excit.), ΔHR, deuterium isotope effects; Rate constantProduct distributionThermodynamic data;
参考文献
Liebigs Annales, , # 10 p. 1529 - 1532
反应条件
potassium fluoride; bis(benzonitrile)palladium(II) dichloride in water; N,N-dimethyl-formamide T=20 - 100°C; 24.05 h;
参考文献
Zhang, Xiaoxia; Larock, Richard C.
Tetrahedron, 2010 , vol. 66, # 24 p. 4265 - 4277
反应条件
1: 99 percent / triethylamine / benzene / 1 h / Heating
2: 0.630 g / methanesulfonic acid / ethanol; diethyl ether / 24 h / Ambient temperature
3: 0.25 g / DDQ / diethyl ether / 2 h / Heating
View Scheme
参考文献
Chung, Ying-Sheng; Kruk, Henry; Barizo, Ophelia M.; Katz, Morris; Lee-Ruff, Edward
Journal of Organic Chemistry, 1987 , vol. 52, # 7 p. 1284 - 1288
