1165952-91-9合成路线 （共 295 条）
反应条件
boron trifluoride diethyl etherate in benzene
1 h; Reflux;
参考文献
THE TRUSTEES OF COLUMBIA UNIVERSITY IN THE CITY OF NEW YORK; SAMES, Dalibor; LI, Xiaoguang; LI, Shu; KRUEGEL, Andrew; KARPOWICZ, Richard; CARRERA, Ignacio; RAKSHIT, Souvik
Patent: WO2013/28999 A1, 2013 ;
Location in patent: Page/Page column 76; 77 ;
反应条件
bis(acetylacetonato) palladium; triethylaluminum; triphenylphosphine
参考文献
Dzhemilev,U.M. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1979 , vol. 28, p. 2512 - 2516
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1979 , vol. 28, # 12 p. 2702 - 2706
反应条件
in diethyl ether
T=-78°C; 72 h;
参考文献
Hart, Terence W.; Haszeldine, Robert N.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1544 - 1550
参考文献
Hart, Terence W.; Haszeldine, Robert N.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1544 - 1550
反应条件
T=-78°C; 72 h; Further byproducts given;
参考文献
Hart, Terence W.; Haszeldine, Robert N.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1544 - 1550
反应条件
T=-78°C; 72 h; other N-halogenoamines; MechanismProduct distribution;
参考文献
Hart, Terence W.; Haszeldine, Robert N.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1544 - 1550
反应条件
in diethyl ether
T=-78°C; 72 h;
参考文献
Hart, Terence W.; Haszeldine, Robert N.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1544 - 1550
反应条件
potassium hydroxide; palladium on activated charcoal
Yield given. Multistep reaction;
参考文献
Haszeldine, R. N.; Tipping, A. E.; Valentine, R. H.
Journal of Fluorine Chemistry, 1982 , vol. 21, p. 329 - 334
反应条件
1: 30 percent / 72 h / -78 °C
2: 1.) sodium isopropoxide / 2.) palladium-charcoal / 1.) diglyme, 160 deg C, 1 h, 2.) 190 deg C
View Scheme
参考文献
Hart, Terence W.; Haszeldine, Robert N.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1544 - 1550
反应条件
2,4,6-triphenylpyrylium-tetrafluoroborate in dichloromethane
0.833333 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Mlcoch, Jiri; Steckhan, Eberhard
Angewandte Chemie, 1985 , vol. 97, # 5 p. 429 - 431
