1165952-91-9合成路线 （共 295 条）
反应条件
in neat (no solvent)
T=120°C; Diels-Alder Cycloaddition; 48 h; Schlenk techniqueInert atmosphere;
参考文献
Xu, Xunfu; Chen, Hu; Wang, Yulei; Gao, Yuxing; Tang, Guo; Zhao, Yufen
RSC Advances, 2014 , vol. 4, # 28 p. 14740 - 14743
反应条件
in chloroform; water; isopropyl alcohol
T=0°C; Cycloaddition; 3 h;
参考文献
Hall, Adrian; Bailey, Patrick D.; Rees, David C.; Rosair, Georgina M.; Wightman, Richard H.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 3 p. 329 - 343
反应条件
1: benzenesulphinic acid sodium salt With polystyrene-supported-SeCl in N,N-dimethyl-formamide
T=20°C; 6 h; solid-phase reaction;
2: cyclohexa-1,3-diene With boron trifluoride diethyl etherate in dichloromethane
T=20°C; 40 h;
3: With dihydrogen peroxide in tetrahydrofuran
T=20°C; 2 h;
参考文献
Qian; Huang
Synlett, 2001 , # 12 p. 1913 - 1916
反应条件
boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid in dichloromethane
Ambient temperature1) 17.5 h, 2) 15 min; Yield given;
参考文献
Baeckvall, Jan-E.; Najera, Carmen; Yus, Miguel
Tetrahedron Letters, 1988 , vol. 29, # 12 p. 1445 - 1448
反应条件
in neat (no solvent)
under N2, educts heated at 90°C; filtered, washed with Et2O; X-ray anal.;
参考文献
Veith, M.; Toellner, F.
Journal of Organometallic Chemistry, 1983 , vol. 246, # 3 p. 219 - 226
反应条件
(-)-(R)-N-Methyl-N-(1-phenylethylamino)diphenylphosphine; bis(1,5-cyclooctadiene)nickel (0); diethylaluminium chloride
T=-70°C; P=9120 Torr; 6 h; other optically active aminophosphines, range of temp.: 0 < T <-70 degC), var. P/Ni ratios; object of study: optical yield; Product distribution;
参考文献
Buono, Gerard; Peiffer, Gilbert; Mortreux, Andre; Petit, Francis
Journal of the Chemical Society, Chemical Communications, 1980 , # 20 p. 937 - 939
反应条件
lithium acetate-d3 in acetone
react. of palladium complex with diene in acetic acid-d4 and acetone-d6 in the presence of lithium acetate-d3; not isolated, detected by NMR;
参考文献
Cotton, Hanna K.; Verboom, Renzo C.; Johansson, Lars; Plietker, Bernd J.; Baeckvall, Jan-E.
Organometallics, 2002 , vol. 21, # 16 p. 3367 - 3375
反应条件
triethylamine in methanol
Irradiation;
参考文献
Quadrelli; Mella; Caramella
Tetrahedron Letters, 1999 , vol. 40, # 4 p. 797 - 800
反应条件
in methanol
5 h; Irradiation;
参考文献
Quadrelli; Mella; Caramella
Tetrahedron Letters, 1999 , vol. 40, # 4 p. 797 - 800
参考文献
Seyferth,D.; Paetsch,J.D.H.
Journal of Organic Chemistry, 1969 , vol. 34, # 5 p. 1483 - 1484
