1165952-91-9合成路线 （共 295 条）
反应条件
sodium perchlorate in water; acetonitrile
(electrolysis);
参考文献
Baltes,H. et al.
Chemische Berichte, 1979 , vol. 112, p. 807 - 817
反应条件
1: 75 percent / KO-t-Bu / pentane / 1.) -20 deg C, 1 h; 2.) room temp., 20 h
2: 40 percent / KO-t-Bu / dimethylsulfoxide / 0.5 h
View Scheme
参考文献
Davalian, Dariush; Garratt, Peter J.; Koller, Wolfgang; Mansuri, Muzammil M.
Journal of Organic Chemistry, 1980 , vol. 45, # 21 p. 4183 - 4193
反应条件
bismuth trifluoromethanesulphonate; [Cu(I)(CH3CN)4]PF6; 1,2-bis-(diphenylphosphino)ethane in 1,4-dioxane
T=100°C; 12 h;
参考文献
Qin, Hongbo; Yamagiwa, Noriyuki; Matsunaga, Shigeki; Shibasaki, Masakatsu
Journal of the American Chemical Society, 2006 , vol. 128, # 5 p. 1611 - 1614
反应条件
1: in toluene
T=150°C; Diels-Alder reaction; 1 h; Microwave irradiationInert atmosphere;
2: With dihydrogen peroxide; triethylamine in tetrahydrofuran
T=0 - 20°C; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Sarotti, Ariel M.; Pisano, Pablo L.; Pellegrinet, Silvina C.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 22 p. 5069 - 5073
反应条件
2,3-dimercapto-succinic acid; ozone
1) -78 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Griesbaum, Karl; Jung, In Chang; Mertens, Henri
Journal of Organic Chemistry, 1990 , vol. 55, # 24 p. 6024 - 6027
反应条件
sodium naphthalenide in tetrahydrofuran
参考文献
Weidenbruch, Manfred; Schaefer, Annemarie; Thom, Karl Ludwig
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1983 , vol. 38, # 12 p. 1695 - 1696
反应条件
2: N2H4, KOH, diethylene glycol
3: H2 / Pt
View Scheme
参考文献
Petit,F. et al.
Bulletin de la Societe Chimique de France, 1972 , p. 747 - 752
反应条件
1: m-chloroperbenzoic acid / CH2Cl2 / 2 h / 20 °C
View Scheme
参考文献
Newcomb, Martin; Lansakara-P, Dharmika S. P.; Kim, Hye-Yeong; Chandrasena, R. Esala P.; Lippard, Stephen J.; Beauvais, Laurance G.; Murray, Leslie J.; Izzo, Viviana; Hollenberg, Paul F.; Coon, Minor J.
Journal of Organic Chemistry, 2007 , vol. 72, # 4 p. 1128 - 1133
参考文献
Danheiser, Rick L.; Martinez-Davila, Carlos; Auchus, Richard J.; Kadonaga, James T.
Journal of the American Chemical Society, 1981 , vol. 103, # 9 p. 2443 - 2446
参考文献
Leivers, Martin; Tam, Iris; Groves, Kevin; Leung, David; Xie, Yuli; Breslow, Ronald
Organic Letters, 2003 , vol. 5, # 19 p. 3407 - 3409
