1165952-91-9合成路线 (共 295 条)
反应条件
hydrogen; palladium on activated charcoal
1) CH2Cl2, 2) EE, 45 psi; Yield given. Multistep reaction;
参考文献
Nelsen, Stephen F.; Petillo, Peter A.; Chang, Hao; Frigo, Timothy B.; Dougherty, Dennis A.; Kaftory, Menahem
Journal of Organic Chemistry, 1991 , vol. 56, # 18 p. 613 - 618
反应条件
Rh4(CO)14; hydrogen in hexane
T=19.85°C; Hydroformylation; reaction was studied by in-situ high-pressure IR spectroscopy; Product distribution;
参考文献
Liu, Guowei; Garland, Marc
Journal of Organometallic Chemistry, 2000 , vol. 608, # 1-2 p. 76 - 85
反应条件
1: HCl / -8 °C
2: diethyl ether
View Scheme
参考文献
Berlande
Bulletin de la Societe Chimique de France, 1942 , vol. <5> 9, p. 644,651, 652
反应条件
oxygen
T=307.9°C; 0.0463889 h; variation of temperature and time; Product distributionMechanismRate constant;
参考文献
Mulder, Peter; Louw, Robert
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 1135 - 1142
反应条件
tin(ll) chloride in tetrahydrofuran
12 h; Ambient temperature; Yield given;
参考文献
Grobe, Joseph; Van, Duc Le; Schulze, Joachim
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1985 , vol. 40, # 12 p. 1753 - 1755
反应条件
bis(1,5-cyclooctadiene)nickel (0); diethylaluminium chloride; triphenylphosphine in toluene
T=50°C; 48 h; other ligands, var. P/Ni and Al/Ni ratios, var. reaction times; Product distribution;
参考文献
Cros, Philippe; Triantaphylides, Christian; Buono, Gerard
Journal of Organic Chemistry, 1988 , vol. 53, # 1 p. 185 - 187
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
T=20°C; 24 h; Product distribution; Further Variations:ReagentsTemperatures;
参考文献
Utsunomiya, Masaru; Kawatsura, Motoi; Hartwig, John F.
Angewandte Chemie - International Edition, 2003 , vol. 42, # 47 p. 5865 - 5868
反应条件
in toluene
T=60°C; 6 h; other H-acceptors; Mechanism;
参考文献
Gerres, Thomas; Heesing, Albert
Chemische Berichte, 1992 , vol. 125, # 6 p. 1431 - 1438
反应条件
2,3-dimercapto-succinic acid; ozone
1) methanol, -78 deg C; Yield given. Multistep reaction;
参考文献
Griesbaum, Karl; Jung, In Chang; Mertens, Henri
Journal of Organic Chemistry, 1990 , vol. 55, # 24 p. 6024 - 6027
反应条件
tetrakis(triphenylphosphine) palladium(0); trifluoroacetic acid in toluene
T=20°C; 24 h;
参考文献
Loeber; Kawatsura; Hartwig
Journal of the American Chemical Society, 2001 , vol. 123, # 18 p. 4366 - 4367