1165952-91-9合成路线 (共 295 条)
反应条件
Multi-step reaction with 2 steps 1: 99 percent / triethylamine / benzene / 1 h / Heating2: 0.630 g / methanesulfonic acid / ethanol; diethyl ether / 24 h / Ambient temperature
参考文献
Chung, Ying-Sheng; Kruk, Henry; Barizo, Ophelia M.; Katz, Morris; Lee-Ruff, Edward Journal of Organic Chemistry, 1987 , vol. 52, # 7 p. 1284 - 1288
反应条件
Multi-step reaction with 2 steps 1: 99 percent / triethylamine / benzene / 1 h / Heating2: 0.45 g / methanesulfonic acid / ethanol; diethyl ether / 24 h / Ambient temperature
参考文献
Chung, Ying-Sheng; Kruk, Henry; Barizo, Ophelia M.; Katz, Morris; Lee-Ruff, Edward Journal of Organic Chemistry, 1987 , vol. 52, # 7 p. 1284 - 1288
反应条件
With peracetic acid; osmium(III) chloride in dichloromethane; ethyl acetate; acetonitrile 3 h; Ambient temperature;
参考文献
Murahashi, Sun-Ichi; Naota, Takeshi; Hanaoka, Hidenori Chemistry Letters, 1993 , # 10 p. 1767 - 1770
反应条件
Multi-step reaction with 6 steps 1: oxygen; 5,15,10,20-tetraphenylporphyrin / tetrachloromethane / 5.5 h / 0 °C / Sun lamp irradiation2: 5,10,15,20-tetraphenyl-21H,23H-porphine Co(II) / 2.5 h / 25 °C / Inert atmosphere3: dilithium tetrabromocuprate / tetrachloromethane; acetonitrile / 1 h / 25 °C4: toluene-4-sulfonic acid / dichloromethane / 2 h / 0 °C5: tetra-(n-butyl)ammonium iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 2 h / Reflux6: oxygen; 5,15,10,20-tetraphenylporphyrin / tetrachloromethane / 7.5 h / Sun lamp irradiation
参考文献
Paddock, Victoria L.; Phipps, Robert J.; Conde-Angulo, Almudena; Blanco-Martin, Araceli; Giro-Manas, Carles; Martin, Laetitia J.; White, Andrew J. P.; Spivey, Alan C. Journal of Organic Chemistry, 2011 , vol. 76, # 5 p. 1483 - 1486
反应条件
With di-tert-butyl peroxide in benzene T=21.9°C; Irradiationexcited at 337.1 nm; Rate constant;
参考文献
Effio, A.; Griller, D.; Ingold, K. U.; Scaiano, J. C.; Sheng, S. J. Journal of the American Chemical Society, 1980 , vol. 102, # 19 p. 6063 - 6068