1165952-91-9合成路线 （共 295 条）
反应条件
hydrogenchloride; p-NO2-benzenesulfonyl azide; hydroquinone 1.) benzene, 90 deg C, 21 h; 2.) aq. ethanol, r. t., 3 d; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 46, # 2 p. 330 - 335
反应条件
2,4,6-triphenylpyrylium-tetrafluoroborate in dichloromethane 0.833333 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Mlcoch, Jiri; Steckhan, Eberhard
Angewandte Chemie, 1985 , vol. 97, # 5 p. 429 - 431
参考文献
Harland, Philip A.; Hodge, Philip
Synthesis, 1982 , # 3 p. 223 - 225
反应条件
1: 250 °C 2: peroxyacetic acid; chloroform View Scheme
参考文献
Walborsky; Loncrini
Journal of the American Chemical Society, 1954 , vol. 76, p. 5396,5399
反应条件
lithium perchlorate in dichloromethane 3 h; Ambient temperature;
参考文献
Reetz; Gansauer
Tetrahedron, 1993 , vol. 49, # 27 p. 6025 - 6030
反应条件
Pd(OBz)2 in acetone T=21.1°C; optical yield given as percent dediastereoselective reaction;
参考文献
Eastgate, Martin D.; Buono, Frederic G.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 32 p. 5958 - 5961
反应条件
palladium diacetate in acetone T=25 - 40°C; Inert atmosphere; MechanismThermodynamic data; Reagent/catalyst; diastereoselective reaction;
参考文献
Eastgate, Martin D.; Buono, Frederic G.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 32 p. 5958 - 5961
反应条件
in acetone T=20°C; diastereoselective reaction;
参考文献
Eastgate, Martin D.; Buono, Frederic G.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 32 p. 5958 - 5961
反应条件
1: toluene-4-sulfonic acid / toluene / 24 h / Reflux 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 12 h / Inert atmosphere; Reflux View Scheme
参考文献
Idemitsu Kosan Co., Ltd.; ITO, Hirokatsu; KAWAMURA, Masahiro; KAWAMURA, Yuichiro; MIZUKI, Yumiko; SAITO, Hiroyuki
Patent: EP2644607 A1, 2013 ;
反应条件
anschliessend mit wss. NaOH behandeln;
参考文献
Weisz, Adrian; Mandelbaum, Asher
Journal of Organic Chemistry, 1988 , vol. 53, # 25 p. 5812 - 5815
