1165952-91-9合成路线 (共 295 条)
反应条件
hydrogen; rhodium 1.) from -196 deg C to RT, 2.) toluene, 50 deg C, 48 h, 70 atm; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Salvadori, Piero; Vitulli, Giovanni; Raffaelli, Andrea; Lazzaroni, Raffaello
Journal of Organometallic Chemistry, 1983 , vol. 258, # 3 p. 351 - 356
反应条件
trimethylamine-N-oxide; (Ipc)2BH 1.) -25 deg C, 12 h; 2.) 0 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Brown, Herbert C.; Jadhav, Prabhakar K.; Bhat, Krishna S.
Journal of the American Chemical Society, 1985 , vol. 107, # 8 p. 2564 - 2565
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane); hydroxide; dihydrogen peroxide 1.) THF, r.t., 48 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Zaidlewicz, Marek; Meller, Jerzy
Tetrahedron Letters, 1997 , vol. 38, # 41 p. 7279 - 7282
反应条件
sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide other cyclic dienes and hydroborating agents; Product distribution;
参考文献
Brown, Herbert C.; Bhat, Krishna S.
Journal of Organic Chemistry, 1986 , vol. 51, # 4 p. 445 - 449
反应条件
1: With sulfur chloride pentafluoride; triethyl borane in hexane T=-40 - 20°C; 1.08333 h; 2: With KMnO4/alumina T=0°C; 1 h;
参考文献
UNIVERSITY OF FLORIDA
Patent: WO2004/11422 A1, 2004 ;
Location in patent: Page 9 ;
反应条件
in diethyl ether Irradiation (UV/VIS);
参考文献
Fischer, E. O.; Muller, J.; Kuzel, P.
Revue de Chimie, Academie de la Republique Populaire Roumaine, 1962 , vol. 7, p. 827 - 834
Full Text Show Details
Gmelin Handbook: Cr: Org.Verb., 1.1.1.1.3, page 10 - 13
反应条件
in benzene T=120°C; 72 h;
参考文献
Tetrahedron, , vol. 63, # 18 p. 3790 - 3799
反应条件
T=500°C; P=1 - 5 Torr;
参考文献
Reinecke, Manfred G.; Newsom, James G.; Chen, Lao-Jer
Journal of the American Chemical Society, 1981 , vol. 103, # 10 p. 2760 - 2769
反应条件
1-hexadecyl-3-methylimidazolium chloride/MCM-48 in toluene T=65°C; Diels-Alder reaction; 72 h; Title compound not separated from byproducts.;
参考文献
Tetrahedron Letters, , vol. 49, # 29-30 p. 4546 - 4549
反应条件
T=200°C; Reagiert analog mit α-Terpinen;
参考文献
Alder; Rickert
Justus Liebigs Annalen der Chemie, 1936 , vol. 524, p. 180,187