1165952-92-0合成路线 (共 138 条)
参考文献
Kiso,Y. et al.
Journal of Organometallic Chemistry, 1973 , vol. 50, p. 297 - 310
反应条件
1: 52 percent / epoxidation
2: 80 percent / lithium aluminum hydride
3: 72 percent / pyridinium chlorochromate, pyridine / CH2Cl2 / 2 h / 5 °C
View Scheme
参考文献
Dzingeleski; Blotny; Pollack
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1019 - 1023
反应条件
Nitrous oxide
T=250°C; 5 h; pressure;
参考文献
Starokon; Dubkov; Babushkin; Parmon; Panov
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 2-3 p. 268 - 274
反应条件
1: benzene; triethylamine / 10 h / 0 °C
2: Br2 / CCl4 / 0.75 h / 0 °C
3: 57 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / tetrahydrofuran / 20 °C
View Scheme
参考文献
Christl, Manfred; Mattauch, Brigitte
Chemische Berichte, 1985 , vol. 118, # 9 p. 4203 - 4223
反应条件
in chloroform; triethylamine
T=60°C; Title compound not separated from byproducts;
参考文献
Christl, Manfred; Mattauch, Brigitte
Chemische Berichte, 1985 , vol. 118, # 9 p. 4203 - 4223
反应条件
T=100°C; 0.5 h; Product distribution;
参考文献
Myers, Andrew G.; Kuo, Elaine Y.; Finney, Nathaniel S.
Journal of the American Chemical Society, 1989 , vol. 111, # 20 p. 8057 - 8059
反应条件
T=90°C; Addition; Myers-Saito cycloaromatization; hydrogenation; 24 h; Product distribution;
参考文献
Hughes, Thomas S.; Carpenter, Barry K.
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 11 p. 2291 - 2298
反应条件
Irradiation; Product distribution;
参考文献
Hawari, J. A.; Davis, S.; Engel, P. S.; Gilbert, B. C.; Griller, D.
Journal of the American Chemical Society, 1985 , vol. 107, # 16 p. 4721 - 4724