1165952-92-0合成路线 (共 138 条)
反应条件
hydrogenchloride; ozone -40 deg C, then ca. 30 min reflux;
参考文献
Mittelbach, Martin; Poklukar, Norbert; Junek, Hans
Liebigs Annalen der Chemie, 1990 , # 2 p. 185 - 188
反应条件
in acetonitrile 10 h; Inert atmosphereIrradiation; Kinetics;
参考文献
Samadi, Abdelouahid; Martinez, Luis A.; Miranda, Miguel A.; Morera, Isabel M.
Photochemistry and Photobiology, 2001 , vol. 73, # 4 p. 359 - 365
反应条件
1.1: I2 / tetrahydrofuran / 4 h / -20 °C 1.2: 51 percent / tetrahydrofuran / 1.5 h / Heating 2.1: 88 percent / aq. KOH / 1 h / Heating 3.1: 90 percent / Et3N; DMAP / CH2Cl2 / 50 h / 20 °C View Scheme
参考文献
O'Brien, Peter; Pilgram, Christopher D.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 3 p. 523 - 534
反应条件
mercury(II) diacetate 168 h;
参考文献
Kleinpeter, Erich; Thielemann, Joerg
Tetrahedron, 2007 , vol. 63, # 37 p. 9071 - 9081
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Beger, J.; Thomas, B.; Vogel, T.; Lang, R.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 3 p. 447 - 453
反应条件
hydrogen; (.eta.3-C3H5)Co[P(OMe)3]3 24 h; Ambient temperature;
参考文献
Journal of the American Chemical Society, , vol. 103, # 3 p. 556 - 564
反应条件
hydrogen; OsH3Cl(CO)(PiPr3)2 in isopropyl alcohol T=60°C; P=750.06 Torr; 0.0833333 h; Title compound not separated from byproducts;
参考文献
Esteruelas, Miguel A.; Sola, Eduardo; Oro, Luis A.; Meyer, Uwe; Werner, Helmut
Angewandte Chemie, 1988 , vol. 100, # 11 p. 1621 - 1622
反应条件
niobium bromide; zinc in N,N-dimethyl-formamide T=60°C; 4.5 h; hydrogen transfer reaction; also with deuterium-labelled compounds; var. conc. of Ni; MechanismProduct distributionRate constant;
参考文献
Chemische Berichte, , vol. 121, p. 1133 - 1136
参考文献
Linstead et al.
Nature (London, United Kingdom), 1952 , vol. 169, p. 100
反应条件
Catalyst M-Chromium oxide in benzene T=90°C; 2 h; var. of catalyst, solvent; Product distribution;
参考文献
Heesing, Albert; Laue, Hans-Joachim
Chemische Berichte, 1986 , vol. 119, # 4 p. 1232 - 1243