1165952-92-0合成路线 （共 138 条）
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane 2 h; Cooling with ice;
参考文献
Cavdar, Huseyin; Saracoglu, Nurullah
European Journal of Organic Chemistry, 2008 , # 27 p. 4615 - 4621
反应条件
in dichloromethane; water T=-15 - -10°C; 23 h; Inert atmosphereMolecular sieve;
参考文献
Durie, Alastair J.; Slawin, Alexandra M. Z.; Lebl, Tomas; Kirsch, Peer; O'Hagan, David
Chemical Communications, 2012 , vol. 48, # 77 p. 9643 - 9645
反应条件
1.1: 100 percent / SO2Cl2 / CCl4 / 2 h / 20 °C 2.1: 96.4 percent / SF5Cl; Et3B / CH2Cl2; hexane / 4 h / -30 - -20 °C 3.1: 79 percent / NaOEt / ethanol / 0.25 h / 20 °C 4.1: 93.7 percent / NBS; H2SO4; TFA / 48 h / 20 °C 5.1: H2SO4; TFA; HNO3 / 48 h / 20 °C 5.2: 0.38 g / Fe; HCl / ethanol / 2 h / 90 - 95 °C View Scheme
参考文献
Sergeeva, Tatiana A.; Dolbier Jr., William R.
Organic Letters, 2004 , vol. 6, # 14 p. 2417 - 2419
反应条件
ruthenacarborane 3 T=60°C; 4 h;
参考文献
Demonceau; Saive; De Froidmont; Noels; Hubert; Chizhevsky; Lobanova; Bregadze
Tetrahedron Letters, 1992 , vol. 33, # 15 p. 2009 - 2012
反应条件
trichlorosilane in N-dodecane T=250°C; 4 h; Inert atmosphere; TemperatureTime;
参考文献
Journal of Organometallic Chemistry, , vol. 724, p. 40 - 44
反应条件
tetrabutyl-ammonium chloride; zinc(II) chloride; bis(dibenzylideneacetone)-palladium(0) in acetonitrile T=100°C; 24 h;
参考文献
Larock, Richard C.; Wang, Yao; Dong, Xiaoyang; Yao, Tuanli
Tetrahedron, 2005 , vol. 61, # 48 p. 11427 - 11439
反应条件
1: 63 percent / O2, TPP / CH2Cl2 / 48 h / Ambient temperature; Irradiation 2: 40 percent / LiAlH4 / tetrahydrofuran / 1 h / Ambient temperature; other reagent, solvent 3: 67 percent / pyridine / 6 h / Ambient temperature 4: 66 percent / KMnO4, MgSO4 / H2O / 15 h / -5 °C 5: 72 percent / pyridine / 6 h / Ambient temperature 6: 132 mg / NH3 / methanol / 2 h View Scheme
参考文献
Salamci; Secen; Sutbeyaz; Balci
Journal of Organic Chemistry, 1997 , vol. 62, # 8 p. 2453 - 2457
反应条件
hydrogenchloride; ozone -40 deg C, then ca. 30 min reflux; Yields of byproduct given;
参考文献
Liebigs Annalen der Chemie, , # 2 p. 185 - 188
反应条件
in pentane T=20°C; 1.5 h; Irradiation; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 103, # 24 p. 7299 - 7304
反应条件
hydrogenchloride; ozone -40 deg C, then ca. 30 min reflux;
参考文献
Mittelbach, Martin; Poklukar, Norbert; Junek, Hans
Liebigs Annalen der Chemie, 1990 , # 2 p. 185 - 188
