1165952-92-0合成路线 （共 138 条）
反应条件
in 1,2,2-trifluoro-trichloroethane T=25°C; Rate constant;
参考文献
Banks, Jeffrey T.; Ingold, Keith U.; Della, Ernest W.; Walton, John C.
Tetrahedron Letters, 1996 , vol. 37, # 44 p. 8059 - 8060
反应条件
hydrogenchloride; ozone -40 deg C, then ca. 30 min reflux;
参考文献
Liebigs Annalen der Chemie, , # 2 p. 185 - 188
反应条件
in water; acetic acid
参考文献
Bird,C.W. et al.
Journal of the Chemical Society, 1963 , p. 410 - 421
参考文献
Cornubert; Rio; Senechal
Bulletin de la Societe Chimique de France, 1955 , p. 46,50
Full Text Show Details
Sakashita
Nippon Kagaku Zasshi, 1959 , vol. 80, p. 972,973
Chem.Abstr., 1960 , p. 2008
反应条件
T=105°C; P=19123.2 Torr; Hydrieren des Reaktionsprodukts an Palladium/Kohle in Aethylacetat;
参考文献
Hofmann et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 992,995
反应条件
Rh(acetylacetonate)-(CO)(PPh3); hydrogen; triphenylphosphine T=80°C; P=7600 Torr; 3 h;
参考文献
Trzeciak, Anna M.; Ziolkowski, Jozef J.
Journal of Organometallic Chemistry, 1994 , vol. 479, # 1-2 p. 213 - 216
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Beger, J.; Thomas, B.; Vogel, T.; Lang, R.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 3 p. 447 - 453
反应条件
1: 100 percent / SO2Cl2 / CCl4 / 2 h / 20 °C 2: 96.4 percent / SF5Cl; Et3B / CH2Cl2; hexane / 4 h / -30 - -20 °C 3: 79 percent / NaOEt / ethanol / 0.25 h / 20 °C 4: 87 percent / HNO3; H2SO4; TFA / 24 h / 0 - 20 °C View Scheme
参考文献
Sergeeva, Tatiana A.; Dolbier Jr., William R.
Organic Letters, 2004 , vol. 6, # 14 p. 2417 - 2419
反应条件
1: 100 percent / SO2Cl2 / CCl4 / 2 h / 20 °C 2: 96.4 percent / SF5Cl; Et3B / CH2Cl2; hexane / 4 h / -30 - -20 °C 3: 79 percent / NaOEt / ethanol / 0.25 h / 20 °C 4: 87 percent / HNO3; H2SO4; TFA / 24 h / 0 - 20 °C 5: 81 percent / Fe; aq. HCl / ethanol / 2 h / 95 °C View Scheme
参考文献
Organic Letters, , vol. 6, # 14 p. 2417 - 2419
反应条件
Hydrieren an Palladium in Aceton, Erwaermen mit aethanol. Kalilauge und mit Acetylchlorid;
参考文献
Diels; Alder
Justus Liebigs Annalen der Chemie, 1931 , vol. 490, p. 257,263
