1-[6-(氯乙酰基)-1H-吲哚-1-基]-2,2-二甲基-1-丙酮合成路线 （共 7 条）
反应条件
aluminium trichloride in 1,2-dichloro-ethane T=20°C;
参考文献
Nakatsuka, Shin-ishi; Teranishi, Katsunori; Goto, Toshio
Tetrahedron Letters, 1994 , vol. 35, # 17 p. 2699 - 2700
反应条件
1: 1.) 60percent NaH / 1.) DMF, 0 deg C, 15 min, 2.) DMF, 4 deg C, 15 min 2: AlCl3 / 1.) 1,2-dichloroethane, 0 deg C, 20 min then 20 deg C, 2.) 1,2-dichloroethane, 20 deg C, 15 min View Scheme
参考文献
Teranishi; Nakatsuka; Goto
Synthesis, 1994 , # 10 p. 1018 - 1020
反应条件
1: 1.) 60percent NaH / 1.) DMF, 0 deg C, 15 min, 2.) DMF, 4 deg C, 15 min 2: AlCl3 / 1.) 1,2-dichloroethane, 0 deg C, 20 min then 20 deg C, 2.) 1,2-dichloroethane, 20 deg C, 15 min View Scheme
参考文献
Teranishi; Nakatsuka; Goto
Synthesis, 1994 , # 10 p. 1018 - 1020
反应条件
aluminium trichloride 1.) 1,2-dichloroethane, 0 deg C, 20 min then 20 deg C, 2.) 1,2-dichloroethane, 20 deg C, 15 min; Yield given. Multistep reaction;
参考文献
Teranishi; Nakatsuka; Goto
Synthesis, 1994 , # 10 p. 1018 - 1020
反应条件
1: 80 percent / m-CPBA (80percent), Na2HPO4 / CH2Cl2 / 1 h / 20 °C 2: 96 percent / 15percent aq. NaSMe / methanol / 2 h / 20 °C 3: 68 percent / 60percent NaH / dimethylformamide / 0.17 h / -20 °C View Scheme
参考文献
Teranishi; Nakatsuka; Goto
Synthesis, 1994 , # 10 p. 1018 - 1020
反应条件
disodium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid in dichloromethane T=20°C; 1 h;
参考文献
Teranishi; Nakatsuka; Goto
Synthesis, 1994 , # 10 p. 1018 - 1020
反应条件
1: 80 percent / m-CPBA (80percent), Na2HPO4 / CH2Cl2 / 1 h / 20 °C 2: 96 percent / 15percent aq. NaSMe / methanol / 2 h / 20 °C View Scheme
参考文献
Teranishi; Nakatsuka; Goto
Synthesis, 1994 , # 10 p. 1018 - 1020
