反应条件
1: 75 percent / dicyclohexylcarbodiimide; CF3CO2H; pyridine / DMSO / toluene / 10 h / 20 °C
2: 80 percent / tetrahydrofuran / 1 h / -78 - 20 °C
3: 95 percent / TBAF / tetrahydrofuran / 1 h / 20 °C
4: aq. NaIO4 / 0.58 h / 0 - 20 °C
5: 11.4 g / NaBH4; CeCl3*7H2O / methanol / 0.5 h / 0 °C
6: Grubbs' catalyst / CH2Cl2 / 4 h / 24 °C
7: 8.3 g / 4 Angstroem molecular sieves; pyridinium dichromate; AcOH / CH2Cl2 / 12 h / 24 °C
View Scheme
参考文献
Chu; Jin; Baker; Huggins
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 1 p. 9 - 12
