反应条件
1: ethyl-1,4-pentadien-3-yl carbonate With titanium(IV) isopropylate; isopropylmagnesium chloride in diethyl ether
T=-50 - -40°C; 2 h;
2: (E)-cinnamaldehyde in diethyl ether
T=-40 - 0°C; 1 h; Title compound not separated from byproducts;
参考文献
Okamoto, Sentaro; Sato, Fumie
Journal of Organometallic Chemistry, 2001 , vol. 624, # 1-2 p. 151 - 156