N-苄氧羰基甘氨酰-L-苯丙氨酸合成路线 (共 69 条)
反应条件
sodium perchlorate; triethylamine in N,N-dimethyl-formamide T=20°C; Condensation; 2 h;
参考文献
Raydnov, M. G.; Klimenko, L. V.; Mitin, Yu. V.
Russian Journal of Bioorganic Chemistry, 1999 , vol. 25, # 5 p. 283 - 287
Bioorganicheskaya Khimiya, 1999 , vol. 25, # 5 p. 323 - 328
反应条件
sulfur trioxide-N,N-dimethylformamide complex; N,N-dimethyl-formamide anschliessendes Behandeln mit L-Phenylalanin und MgCO3 in H2O;
参考文献
Journal of the Chemical Society, , p. 1398,1403
反应条件
1: H2SO4 / CH2Cl2 2: H2 / Pd-C / ethanol 3: tetraethyl diphosphite / dimethylformamide 4: TsOH / benzene View Scheme
参考文献
Journal of the American Chemical Society, , vol. 82, p. 3359 - 3363
反应条件
1: H2 / Pd-C / ethanol 2: tetraethyl diphosphite / dimethylformamide 3: TsOH / benzene View Scheme
参考文献
Journal of the American Chemical Society, , vol. 82, p. 3359 - 3363
反应条件
4-methyl-morpholine in N-sodium hydroxide; toluene
参考文献
Research Corporation
Patent: US4261884 A1, 1981 ;
反应条件
cross-linked enzyme aggregate of Alcalase; water T=37°C; 16 h; Enzymatic reaction;
参考文献
Nuijens, Timo; Cusan, Claudia; Schepers, Annette C.H.M.; Kruijtzer, John A.W.; Rijkers, Dirk T.S.; Liskamp, Rob M.J.; Quaedflieg, Peter J.L.M.
Journal of Molecular Catalysis B: Enzymatic, 2011 , vol. 71, # 1-2 p. 79 - 84
反应条件
sodium chloride; calcium chloride; trypsin in N,N-dimethyl-formamide T=25°C; pH=8; 3 h; aq. bufferEnzymatic reaction;
参考文献
ChemBioChem, , vol. 13, # 12 p. 1785 - 1790
反应条件
sodium sulfide in water; acetonitrile 3 h; Ambient temperature;
参考文献
Amaral Trigo, M. Joaquina S. A.; Oliveira Santos, M. Isabel A.
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 11B p. 2787 - 2790
反应条件
sodium carbonate T=0 - 20°C; 1.33333 h;
参考文献
Schuemacher; Hoffmann
Synthesis, 2001 , # 2 p. 243 - 246
反应条件
sodium chloride; calcium chloride; trypsin in N,N-dimethyl-formamide T=25°C; pH=8; 2 h; aq. bufferEnzymatic reaction;
参考文献
ChemBioChem, , vol. 13, # 12 p. 1785 - 1790