N-苄氧羰基甘氨酰-L-苯丙氨酸合成路线 (共 69 条)
反应条件
1: 95 percent / Jones' reagent / acetone / 3 h / 0 °C 2: 63 percent / DCC / CH2Cl2 / 10 h / Ambient temperature 3: Jones' reagent View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 535 - 540
反应条件
1: 38 percent / NaHCO3 / CH2Cl2; H2O / Ambient temperature 2: 95 percent / Jones' reagent / acetone / 3 h / 0 °C 3: 63 percent / DCC / CH2Cl2 / 10 h / Ambient temperature 4: Jones' reagent View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 535 - 540
反应条件
1: (i) PCl3, Py, (ii) /BRN= 526877/ 2: aq. NaOH / dioxane View Scheme
参考文献
Chemische Berichte, , vol. 98, p. 2831 - 2836
反应条件
diethyl ether; potassium hydrogencarbonate Behandeln des Reaktionsprodukts mit wss.-aethanol. Natronlauge;
参考文献
Journal of Biological Chemistry, , vol. 134, p. 225,233
Journal of Biological Chemistry, , vol. 170, p. 221,222
反应条件
Ambient temperature;
参考文献
Chung-hsi, Li; Yuen-hwa, Yieh; Yao, Lin; Yong-jun, Lu; Ai-hsueh, Chi; Chi-yi, Hsing
Tetrahedron Letters, 1981 , vol. 22, # 36 p. 3467 - 3470
反应条件
triethylamine in 1,4-dioxane
参考文献
Justus Liebigs Annalen der Chemie, , vol. 684, p. 236 - 242
参考文献
Bulletin of the Chemical Society of Japan, , vol. 40, # 3 p. 656 - 661
反应条件
2-Hydroxypyridine; dicyclohexyl-carbodiimide
参考文献
Journal of pharmaceutical sciences, , vol. 57, # 9 p. 1514 - 1519
反应条件
in N,N-dimethyl-formamide 6 h; Ambient temperature; Yield given;
参考文献
Tetrahedron Letters, , vol. 23, # 37 p. 3831 - 3834
反应条件
(i) cyclohexyl-isobutoxycarbonyl-dimethyl-ammonium fluoroborate, AcOEt, (ii) /BRN= 526877/, Et3N; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 39, p. 1499 - 1503