2-羟基-2-(三氟甲基)-4-戊烯酸甲酯合成路线 (共 3 条)
反应条件
tin(IV) chloride in hexane 1.) -70 deg C, -50 deg C, -10 deg C (2 h);
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, # 1 p. 117 - 121
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 1 p. 127 - 132
反应条件
in diethyl ether T=-50 - 20°C;
参考文献
Tetrahedron, , vol. 52, # 1 p. 143 - 148
反应条件
zinc in ethanol 1) kept 1 h after exothermic start, 2) reflux 0.5 h; Yields of byproduct given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, # 7 p. 1298 - 1303
Zhurnal Organicheskoi Khimii, , vol. 23, # 7 p. 1441 - 1447