6-(2-甲氢吡喃氧基)已基溴化镁合成路线 （共 6 条）
反应条件
iodine in tetrahydrofuran 0.75 h; Heating / reflux;
参考文献
MARTEK BIOSCIENCES CORPORATION; RAMAN, Krishna; TARWADE, Vinod; SALEM, Norman, Jr.
Patent: WO2011/53892 A1, 2011 ;
Location in patent: Page/Page column 45 ;
反应条件
1: aq. HBr; heptane 2: p-TsOH 3: Mg / tetrahydrofuran View Scheme
参考文献
Hahn,S.; Stoilov,I.L.; Tam Ha,T.B.
Journal of the American Chemical Society, 1988 , vol. 110, p. 8117
反应条件
1: p-TsOH 2: Mg / tetrahydrofuran View Scheme
参考文献
Hahn,S.; Stoilov,I.L.; Tam Ha,T.B.
Journal of the American Chemical Society, 1988 , vol. 110, p. 8117
反应条件
magnesium in tetrahydrofuran
参考文献
Hahn,S.; Stoilov,I.L.; Tam Ha,T.B.
Journal of the American Chemical Society, 1988 , vol. 110, p. 8117
反应条件
1: Li2CuCl4 / tetrahydrofuran / 2 h / 0 °C 2: p-toluol sulfonic acid / methanol; H2O / 2 h / 60 °C View Scheme
参考文献
Bestmann; Suess; Vostrowsky
1981 , vol. No. 12, p. 2117 - 2138
反应条件
1: 71 percent / tetrahydrofuran / 0.5 h at 0 deg C, then 3 h at 25 deg C
2: 90 percent / CrO3*Py*HCl / CH2Cl2 / 2 h
3: 90 percent / 5percent HCl / acetone / 48 h
View Scheme
参考文献
Odinokov, V. N.; Botsman, L. P.; Nagaeva, N. A.; Tolstikov, G. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 68 - 70
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 1 p. 80 - 83
