(Z)-3,4,5,4’,-四甲氧基-3’-羟基二苯乙烯合成路线 （共 68 条）
反应条件
1: LiBr, TMSCl / acetonitrile 2: toluene 3: n-BuLi / tetrahydrofuran 4: (n-Bu)4NF / tetrahydrofuran View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 6, # 2 p. 157 - 160
反应条件
1: With FeH(CO)(NO)(PPh3)2; phenyl silane; triethylamine in tetrahydrofuran T=60°C; 2: With tetrabutyl ammonium fluoride in tetrahydrofuran T=0°C; 2 h; Inert atmosphere; optical yield given as percent dediastereoselective reaction;
参考文献
Chemical Communications, , vol. 48, # 44 p. 5419 - 5421
反应条件
sodium hydroxide in N,N-dimethyl-formamide Product distribution / selectivity;
参考文献
WO2007/59118 A1, ;
Page/Page column 27-28 ;
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium hydroxide in ethylene glycol dimethyl ether; water T=100°C; Suzuki-Miyaura cross-coupling; 0.25 h; Inert atmosphereMicrowave irradiation; optical yield given as percent destereoselective reaction;
参考文献
Synlett, , # 17 p. 2789 - 2794
反应条件
quinoline; copper 2 h; Heating; stereoselective reaction;
参考文献
Li, Xiao-Jing; Yang, Liu; Liu, Ying-Qian; Li, Chong
Natural Product Research, 2012 , vol. 26, # 14 p. 1271 - 1277
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran Yield given;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 6, # 2 p. 157 - 160
反应条件
1.1: butyllithium / hexane; tetrahydrofuran / 15 - 20 °C 1.2: 54 percent / hexane; tetrahydrofuran / 1 h / 20 °C 2.1: tetrabutylammonium fluoride / tetrahydrofuran / 0.25 h / 20 °C View Scheme
参考文献
Carbohydrate Research, , vol. 301, # 3-4 p. 95 - 109
反应条件
1.1: 80 percent / toluene 2.1: butyllithium / hexane; tetrahydrofuran / 15 - 20 °C 2.2: 54 percent / hexane; tetrahydrofuran / 1 h / 20 °C 3.1: tetrabutylammonium fluoride / tetrahydrofuran / 0.25 h / 20 °C View Scheme
参考文献
Carbohydrate Research, , vol. 301, # 3-4 p. 95 - 109
反应条件
1: toluene 2: n-BuLi / tetrahydrofuran 3: (n-Bu)4NF / tetrahydrofuran View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 6, # 2 p. 157 - 160
反应条件
1: n-BuLi / tetrahydrofuran 2: (n-Bu)4NF / tetrahydrofuran View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 6, # 2 p. 157 - 160
