1-(5-氯-2,3-二甲氧基苯基)乙醇合成路线 (共 3 条)
反应条件
in diethyl ether T=20°C; 4 h; Reflux;
参考文献
Laboratorios Del. Dr. Esteve, S.A.
Patent: EP2103596 A1, 2009 ;
Location in patent: Page/Page column 50 ;
反应条件
magnesium 2.) ether, benzene, reflux, 6 h; Yield given. Multistep reaction;
参考文献
Kuleshyus, V. A.; Gaidyalis, P. G.; Pyatrauskas, O. Yu.; Daukshas, V. K.
Pharmaceutical Chemistry Journal, 1988 , vol. 22, # 7 p. 551 - 553
Khimiko-Farmatsevticheskii Zhurnal, 1988 , vol. 22, # 7 p. 827 - 830
反应条件
manganese(IV) oxide in chloroform 8 h; Reflux;
参考文献
EP2103596 A1, ;
Page/Page column 50 ;