3-(BOC-氨基)吡啶-5-硼酸频哪醇酯合成路线 （共 3 条）
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in 1,4-dioxane T=100°C; 20 h; Inert atmosphereSealed tube;
参考文献
PETER MACCALLUM CANCER INSTITUTE; SPICER, Julie Ann; DENNY, William Alexander; MILLER, Christian Karl; O'CONNOR, Patrick David; HUTTUNEN, Kristiina; TRAPANI, Joseph A.; HILL, Geoff; ALEXANDER, Kylie
Patent: WO2014/28968 A1, 2014 ;
Location in patent: Page/Page column 102 ;
反应条件
1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.33 h / 20 °C 1.2: 24 h / 20 °C 2.1: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct / 1,4-dioxane / 0.75 h / 120 °C / Inert atmosphere; Microwave irradiation View Scheme
参考文献
WO2011/28741 A1, ;
WO 2011/028741 A1
反应条件
1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.33 h / 20 °C 1.2: 24 h / 20 °C 2.1: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct / 1,4-dioxane / 0.75 h / 120 °C / Inert atmosphere; Microwave irradiation View Scheme
参考文献
WO2011/28741 A1, ;
WO 2011/028741 A1
