2-甲酰基-N-甲基苯甲酰胺合成路线 （共 4 条）
反应条件
hydrogenchloride; sodium tetrahydroborate in ethanol T=0 - 5°C; 2 h;
参考文献
Takeuchi, Hisato; Eguchi, Shoji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2149 - 2154
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine 1.) Et2O, 2.) THF; Yield given. Multistep reaction;
参考文献
Belliotti, Thomas R.; Brink, Wouter A.; Kesten, Suzanne R.; Rubin, John R.; Wustrow, David J.; Zoski, Kim T.; Whetzel, Steven Z.; Corbin, Ann E.; Pugsley, Thomas A.; Heffner, Thomas G.; Wise, Lawrence D.
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 12 p. 1499 - 1502
反应条件
1: With copper(I) bromide in tetrachloromethane; acetonitrile T=20°C; 0.25 h; Inert atmosphere; 2: With N-bromosuccinmide in tetrachloromethane; acetonitrile T=75°C; 12 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 14, # 34 p. 10722 - 10726
反应条件
1: 74 percent / DPPA, Et3N / benzene
2: 65 percent / xylene / Heating
View Scheme
参考文献
Takeuchi, Hisato; Eguchi, Shoji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2149 - 2154
