1,2-二甲基-1,1,2,2-四苯基乙硅烷合成路线 (共 27 条)
反应条件
diphenyl(methyl)silyl chloride; tetra-n-butylammonium perchlorate; copper(l) chloride in ethylene glycol dimethyl ether electrochemical reaction; Yield given. Yields of byproduct given;
参考文献
Chemistry Letters, , # 11 p. 1945 - 1948
反应条件
tetra-n-butylammonium perchlorate; 2,3-dimethyl-buta-1,3-diene in ethylene glycol dimethyl ether electrolysis, electrolytic reduction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 67, # 1 p. 287 - 289
反应条件
in diethyl ether 10 h; Heating;
参考文献
Russian Chemical Bulletin, , vol. 44, # 5 p. 927 - 930
Izvestiya Akademi Nauk, Seriya Khimicheskaya, , # 5 p. 954 - 957
反应条件
aluminium trichloride 1) electrolysis; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 20 p. 2107 - 2108
反应条件
hydrogenchloride; aluminium trichloride in benzene
参考文献
Ernst, Margot; Schenzel, Karla; Jaehn, Anke; Hassler, Karl
Journal of Molecular Structure, 1997 , vol. 412, # 1-2 p. 83 - 95
反应条件
1 Au/TiO2; water in ethyl acetate T=25°C; 1 h; Overall yield = 98 percent;
参考文献
Gryparis, Charis; Stratakis, Manolis
Chemical Communications (Cambridge, United Kingdom), 2012 , vol. 48, # 87 p. 10751 - 10753,3
反应条件
potassium hydride in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide 72 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 44, # 13 p. 4181 - 4196
反应条件
potassium hydride in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide 72 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 44, # 13 p. 4181 - 4196
反应条件
C6H5Br; Na-K (C6H5)2(CH3)SiSi(CH3)(C6H5)2 and Na-K-alloy;;
参考文献
Gmelin Handbook: Si: MVol.C, 113, page 316 - 320
反应条件
bromine in carbon disulfide T=23°C; Rate constant;
参考文献
Monatshefte fuer Chemie, , vol. 112, p. 731 - 742