2-(三甲基硅烷基)乙基beta-吡喃半乳糖苷合成路线 （共 6 条）
反应条件
sodium methylate in methanol 3 h;
参考文献
Jansson, Karl; Ahlfors, Stefan; Frejd, Torbjoern; Kihlberg, Jan; Magnusson, Goeran; et al.
Journal of Organic Chemistry, 1988 , vol. 53, # 24 p. 5629 - 5647
反应条件
1: silver oxide / CH2Cl2 2: sodium hydroxide / methanol View Scheme
参考文献
Jansson, Karl; Ahlfors, Stefan; Frejd, Torbjoern; Kihlberg, Jan; Magnusson, Goeran; et al.
Journal of Organic Chemistry, 1988 , vol. 53, # 24 p. 5629 - 5647
反应条件
1: 84 percent / HgO, HgBr2, CaSO4 / CHCl3 / 48 h / Ambient temperature 2: 90 percent / CH3ONa / methanol / 3 h View Scheme
参考文献
Kajimoto, Tetsuya; Ishioka, Yuichi; Katoh, Takahiro; Node, Manabu
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 22 p. 5736 - 5739
反应条件
trifluorormethanesulfonic acid in dimethyl sulfoxide T=90°C; 48 h; Yield given. Yields of byproduct given;
参考文献
Konradsson, Peter; Roberts, Carmichael; Fraser-Reid, Bert
Recueil des Travaux Chimiques des Pays-Bas, 1991 , vol. 110, # 1 p. 23 - 24
反应条件
in water; tert-butyl alcohol T=50°C; 192 h; β-D-glucosidase;
参考文献
Vic, Gabin; Hastings, Jeremy J.; Crout, David H. G.
Tetrahedron Asymmetry, 1996 , vol. 7, # 7 p. 1973 - 1984
反应条件
4 A molecular sieve; tetrabutylammomium bromide; di(n-butyl)tin oxide 1.) methanol, 2 h , reflux, 2.) benzene, 4 d, 25 - 30 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Murase, Takatoshi; Kartha, K. P. Ravindranathan; Kiso, Makoto; Hasegawa, Akira
Carbohydrate Research, 1989 , vol. 195, # 1 p. 134 - 137
