暂无反应条件数据

1: NaH / tetrahydrofuran / 2 h / 0 °C 2: AcOH / methanol / 6 h / 40 °C 3: imidazole / dimethylformamide / 10 h / Ambient temperature 4: diisobutylaluminum hydride (Dibal) / hexane; diethyl ether / 0.5 h / -20 °C 5: NH2OH*HCl, pyridine / CH2Cl2 / 4 h / Ambient temperature 6: NaOCl / CH2Cl2 / 4 h / Ambient temperature 7: H2, B(OH)3 / 10percent Pd/C / tetrahydrofuran; H2O / 4 h / 760 Torr / Ambient temperature 8: CH3SO2Cl, Et3N / CH2Cl2 / 0.67 h / 0 °C 9: 95 percent / tetrahydrofuran / 12 h / Ambient temperature View Scheme

1: AcOH / methanol / 6 h / 40 °C 2: imidazole / dimethylformamide / 10 h / Ambient temperature 3: diisobutylaluminum hydride (Dibal) / hexane; diethyl ether / 0.5 h / -20 °C 4: NH2OH*HCl, pyridine / CH2Cl2 / 4 h / Ambient temperature 5: NaOCl / CH2Cl2 / 4 h / Ambient temperature 6: H2, B(OH)3 / 10percent Pd/C / tetrahydrofuran; H2O / 4 h / 760 Torr / Ambient temperature 7: CH3SO2Cl, Et3N / CH2Cl2 / 0.67 h / 0 °C 8: 88 percent / tetrahydrofuran / Ambient temperature View Scheme

1: diisobutylaluminum hydride (Dibal) / hexane; diethyl ether / 0.5 h / -20 °C 2: NH2OH*HCl, pyridine / CH2Cl2 / 4 h / Ambient temperature 3: NaOCl / CH2Cl2 / 4 h / Ambient temperature 4: H2, B(OH)3 / 10percent Pd/C / tetrahydrofuran; H2O / 4 h / 760 Torr / Ambient temperature 5: CH3SO2Cl, Et3N / CH2Cl2 / 0.67 h / 0 °C 6: 88 percent / tetrahydrofuran / Ambient temperature View Scheme

1: NaOCl / CH2Cl2 / 4 h / Ambient temperature 2: H2, B(OH)3 / 10percent Pd/C / tetrahydrofuran; H2O / 4 h / 760 Torr / Ambient temperature 3: CH3SO2Cl, Et3N / CH2Cl2 / 0.67 h / 0 °C 4: 88 percent / tetrahydrofuran / Ambient temperature View Scheme

1: NH2OH*HCl, pyridine / CH2Cl2 / 4 h / Ambient temperature 2: NaOCl / CH2Cl2 / 4 h / Ambient temperature 3: H2, B(OH)3 / 10percent Pd/C / tetrahydrofuran; H2O / 4 h / 760 Torr / Ambient temperature 4: CH3SO2Cl, Et3N / CH2Cl2 / 0.67 h / 0 °C 5: 95 percent / tetrahydrofuran / 12 h / Ambient temperature View Scheme

1: diisobutylaluminum hydride (Dibal) / hexane; diethyl ether / 0.5 h / -20 °C 2: NH2OH*HCl, pyridine / CH2Cl2 / 4 h / Ambient temperature 3: NaOCl / CH2Cl2 / 4 h / Ambient temperature 4: H2, B(OH)3 / 10percent Pd/C / tetrahydrofuran; H2O / 4 h / 760 Torr / Ambient temperature 5: CH3SO2Cl, Et3N / CH2Cl2 / 0.67 h / 0 °C 6: 95 percent / tetrahydrofuran / 12 h / Ambient temperature View Scheme

1: NaOCl / CH2Cl2 / 4 h / Ambient temperature 2: H2, B(OH)3 / 10percent Pd/C / tetrahydrofuran; H2O / 4 h / 760 Torr / Ambient temperature 3: CH3SO2Cl, Et3N / CH2Cl2 / 0.67 h / 0 °C 4: 95 percent / tetrahydrofuran / 12 h / Ambient temperature View Scheme

1: H2, B(OH)3 / 10percent Pd/C / tetrahydrofuran; H2O / 4 h / 760 Torr / Ambient temperature 2: CH3SO2Cl, Et3N / CH2Cl2 / 0.67 h / 0 °C 3: 88 percent / tetrahydrofuran / Ambient temperature View Scheme

1: H2, B(OH)3 / 10percent Pd/C / tetrahydrofuran; H2O / 4 h / 760 Torr / Ambient temperature 2: CH3SO2Cl, Et3N / CH2Cl2 / 0.67 h / 0 °C 3: 95 percent / tetrahydrofuran / 12 h / Ambient temperature View Scheme