2,3,5,6-四氟-4-三氟甲基苯甲酰氟合成路线 （共 6 条）
反应条件
potassium fluoride T=200°C; 16 h;
参考文献
Karpov, V. M.; Panteleev, I. V.; Platonov, V. E.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, p. 1932 - 1938
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, p. 2183 - 2191
反应条件
1: 7.09 g / SOCl2, DMF / 3 h / 80 - 110 °C 2: 3.14 g / KF / 16 h / 200 °C View Scheme
参考文献
Karpov, V. M.; Panteleev, I. V.; Platonov, V. E.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, p. 1932 - 1938
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, p. 2183 - 2191
反应条件
1: 1.) SbF5, SiO2, 2.) H2O / 1.) 75 deg C, 4 h 2: 7.09 g / SOCl2, DMF / 3 h / 80 - 110 °C 3: 3.14 g / KF / 16 h / 200 °C View Scheme
参考文献
Karpov, V. M.; Panteleev, I. V.; Platonov, V. E.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, p. 1932 - 1938
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, p. 2183 - 2191
反应条件
water; SbF5 1.) 130 deg C, 10 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Karpov, V. M.; Panteleev, I. V.; Platonov, V. E.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, p. 1932 - 1938
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, p. 2183 - 2191
反应条件
1: 1.) SbF5, 2.) H2O / 1.) 130 deg C, 10 h
2: SOCl2 / dimethylformamide / 3 h / 80 - 110 °C
3: KF / 16 h / 200 °C
View Scheme
参考文献
Karpov, V. M.; Panteleev, I. V.; Platonov, V. E.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, p. 1932 - 1938
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, p. 2183 - 2191
反应条件
water; SbF5
1.) 130 deg C, 10 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Karpov, V. M.; Panteleev, I. V.; Platonov, V. E.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, p. 1932 - 1938
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, p. 2183 - 2191
