N-[9H-芴-9-基甲氧羰基]甘氨酰-L-苯丙氨酸合成路线 （共 7 条）
反应条件
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane
T=0°C; Inert atmosphere;
参考文献
Vishwanatha; Narendra; Chattopadhyay, Basab; Mukherjee, Monika; Sureshbabu, Vommina V.
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2689 - 2702
反应条件
sodium carbonate in 1,4-dioxane
4 h; Ambient temperature;
参考文献
Nichifor, Marieta; Schacht, Etienne H.
Tetrahedron, 1994 , vol. 50, # 12 p. 3747 - 3760
反应条件
sodium hydrogencarbonate in acetone
Ambient temperature;
参考文献
Djedaini-Pilard, Florence; Azaroual-Bellanger, Nathalie; Gosnat, Muriel; Vernet, Delphine; Perly, Bruno
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 4 p. 723 - 730
反应条件
1: N-methylmorpholine; HATU / CH2Cl2
2: 91 percent / silica gel / toluene / 1 h / Heating
View Scheme
参考文献
Jackson, Randy W
Tetrahedron Letters, 2001 , vol. 42, # 31 p. 5163 - 5165
反应条件
1: N-methylmorpholine; HATU / CH2Cl2
2: 91 percent / silica gel / toluene / 1 h / Heating
View Scheme
参考文献
Jackson, Randy W
Tetrahedron Letters, 2001 , vol. 42, # 31 p. 5163 - 5165
反应条件
1: zinc / tetrahydrofuran / 20 °C
2: water; calcium chloride; sodium hydroxide / isopropyl alcohol
View Scheme
参考文献
Ramesh; Raju; Srinivas; Sureshbabu; Vishwanatha; Hemantha
Rapid Communications in Mass Spectrometry, 2011 , vol. 25, # 14 p. 1949 - 1958
反应条件
Multistep reaction.;
参考文献
Ulijn, Rein V.; Bisek, Nicola; Halling, Peter J.; Flitsch, Sabine L.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 8 p. 1277 - 1281
