反应条件
1: trichlorophosphate / N,N-dimethyl-formamide / 1 h / 80 °C
2: sodium azide / N,N-dimethyl-formamide / 22 h / 20 °C
3: hydrogen / palladium 10 on activated carbon / methanol / 23 h / 20 °C
View Scheme
参考文献
Jitsuoka, Makoto; Nagase, Tsuyoshi; Sato, Nagaaki; Tsukahara, Daisuke
Patent: US2011/9622 A1, 2011 ;
