反应条件
1: diethyl (2-((2-bromophenyl)(methyl)amino)-2-oxoethyl)phosphonate With KDMO; palladium diacetate in tetrahydrofuran; n-heptane
T=100°C; 0.166667 h; Microwave irradiationInert atmosphere;
2: formaldehyd in tetrahydrofuran; n-heptane
T=100°C; Horner-Wadsworth-Emmons (HWE) olefination; 0.5 h; Microwave irradiation;
3: With sodium tetrahydroborate in tetrahydrofuran; n-heptane
参考文献
Millemaggi, Alessia; Perry, Alexis; Whitwood, Adrian C.; Taylor, Richard J. K.
European Journal of Organic Chemistry, 2009 , # 18 p. 2947 - 2952
