3-溴-4-甲氧基苯甲腈合成路线 （共 14 条）
反应条件
hydroxylamine hydrochloride; 1-propanephosphonic acid cyclic anhydride; triethylamine in ethyl acetate; N,N-dimethyl-formamide T=100°C;
参考文献
Augustine, John Kallikat; Atta, Rajendra Nath; Ramappa, Balakrishna Kolathur; Boodappa, Chandrakantha
Synlett, 2009 , # 20 p. 3378 - 3382
反应条件
[{RuCl2(p-cymene)}2]; diphenyl acetylene in isopropyl alcohol T=100°C; 16 h; Inert atmosphere; regioselective reaction;
参考文献
Chinnagolla, Ravi Kiran; Pimparkar, Sandeep; Jeganmohan, Masilamani
Chemical Communications, 2013 , vol. 49, # 30 p. 3146 - 3148
反应条件
in DMF (N,N-dimethyl-formamide) T=20°C; 3 - 12 h;
参考文献
US2005/153877 A1, ;
Page/Page column 122 ;
US 20050153877 A1
反应条件
N-bromosuccinmide; K3PO4*7H2O; trimethylsilylazide; copper diacetate in acetonitrile T=80°C; 25 h; Schlenk technique;
参考文献
Zong, Xiaolin; Zheng, Qing-Zhong; Jiao, Ning
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 8 p. 1198 - 1202
反应条件
[{RuCl2(p-cymene)}2]; diphenyl acetylene in isopropyl alcohol T=100°C; 16 h; Inert atmosphere; regioselective reaction;
参考文献
Chemical Communications, , vol. 49, # 30 p. 3146 - 3148
反应条件
oxygen; potassium bromide; potassium nitrate in water; trifluoroacetic acid T=20°C; 48 h; 50-60 deg C, 10 h; Product distribution;
参考文献
Cheprakov, A. V.; Makhon'kov, D. I.; Rodkin, M. A.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 2 p. 217 - 223
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 2 p. 248 - 255
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium; bromine; zinc(II) chloride T=-70°C;
参考文献
Tetrahedron Letters, , vol. 50, # 7 p. 741 - 744
反应条件
in acetonitrile-D3; water-d2 T=35°C; UV-irradiation; Quantum yield;
参考文献
Organic Letters, , vol. 9, # 15 p. 2803 - 2806
反应条件
in acetonitrile-D3; water-d2 T=35°C; UV-irradiation; Kinetics;
参考文献
Journal of Organic Chemistry, , vol. 73, # 5 p. 1925 - 1934
反应条件
Behandeln des Reaktionsprodukts mit Sodaloesung;
参考文献
Journal of the Chemical Society, , vol. 125, p. 1062
