3-溴-4-甲氧基苯甲腈合成路线 （共 14 条）
反应条件
sodium azide; 2-farnesylacetoxyethyltriethylammonium bromide in toluene Heating / reflux;
参考文献
WARNER-LAMBERT COMPANY LLC
Patent: WO2004/14384 A2, 2004 ;
Location in patent: Page/Page column 171-172; 174 ;
WO 2004/014384 A2
反应条件
borane in tetrahydrofuran Reflux;
参考文献
Glaxo Group Limited
Patent: US2009/197871 A1, 2009 ;
Location in patent: Page/Page column 72 ;
US 20090197871 A1
反应条件
1: With n-butyllithium; tri-isopropoxy-borane in tetrahydrofuran; hexane T=-78°C; 1.33333 h; Cooling with acetone-dry ice; 2: With phosphoric acid in tetrahydrofuran; hexane; water T=-78 - 20°C; Cooling with acetone-dry ice;
参考文献
WO2005/121102 A2, ;
Page/Page column 28-29 ;
WO 2005/121102 A2
反应条件
triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride
T=100°C; P=3102.97 Torr; 4 h;
参考文献
Abbott Laboratories
Patent: US2008/287510 A1, 2008 ;
Location in patent: Page/Page column 24-25 ;
