1: 0.16 g / 80percent aq. HOAc / 4.5 h 2: dicyclohexylcarbodiimide / pyridine / 72 h / Ambient temperature 3: 2 M NaOH / 2 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 32, # 2 p. 367 - 374
1: 0.16 g / 80percent aq. HOAc / 4.5 h 2: dicyclohexylcarbodiimide / pyridine / 72 h / Ambient temperature 3: 86 mg / 2 M NaOH / 2 h / Ambient temperature View Scheme
参考文献
Lambert, Robert W.; Martin, Joseph A.; Thomas, Gareth J.; Duncan, Ian B.; Hall, Michael J.; Heimer, Edgar P.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 2 p. 367 - 374
1: 0.16 g / 80percent aq. HOAc / 4.5 h
2: dicyclohexylcarbodiimide / pyridine / 72 h / Ambient temperature
3: 2 M NaOH / 2 h / Ambient temperature
4: H2 / Lindlar catalyst (poisoned)
5: pyridine / 4.5 h
6: pyridine / 24 h
7: 80percent aq. HOAc / 4.5 h
8: dicyclohexylcarbodiimide / pyridine / 72 h / Ambient temperature
9: 2 M NaOH / 2 h / Ambient temperature
View Scheme
参考文献
Lambert, Robert W.; Martin, Joseph A.; Thomas, Gareth J.; Duncan, Ian B.; Hall, Michael J.; Heimer, Edgar P.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 2 p. 367 - 374
1: 0.16 g / 80percent aq. HOAc / 4.5 h
2: dicyclohexylcarbodiimide / pyridine / 72 h / Ambient temperature
3: 2 M NaOH / 2 h / Ambient temperature
4: H2 / Lindlar catalyst (poisoned)
View Scheme
参考文献
Lambert, Robert W.; Martin, Joseph A.; Thomas, Gareth J.; Duncan, Ian B.; Hall, Michael J.; Heimer, Edgar P.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 2 p. 367 - 374
