N-苄基-5-溴-2-糠酰胺合成路线 （共 4 条）
反应条件
in benzene 0.5 h; Heating;
参考文献
Rai, Usha Kumari; Shanker, Birja; Singh, Sujan; Rao, R. Balaji
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 674 - 675
反应条件
4-(N,N-dimethlyamino)pyridine; oligomeric alkyl cyclohexylcarbodiimide in dichloromethane T=20°C;
参考文献
Zhang, Mianji; Vedantham, Punitha; Flynn, Daniel L.; Hanson, Paul R.
Journal of Organic Chemistry, 2004 , vol. 69, # 24 p. 8340 - 8344
反应条件
1: (COCl)2 / CH2Cl2; dimethylformamide / 1.5 h / 0 - 20 °C 2: 15 g / Et3N / tetrahydrofuran / 1 h / 0 - 20 °C View Scheme
参考文献
Crawford, Kenneth R.; Bur, Scott K.; Straub, Christopher S.; Padwa, Albert
Organic Letters, 2003 , vol. 5, # 18 p. 3337 - 3340
反应条件
1: 5-bromofuran-2-carboxylic acid benzylamide With sodium hydroxide; (n-Bu4)HSO4; potassium carbonate in benzene
T=20°C; 1 h;
2: allyl bromide in benzene
T=20°C; 22 h;
参考文献
Crawford, Kenneth R.; Bur, Scott K.; Straub, Christopher S.; Padwa, Albert
Organic Letters, 2003 , vol. 5, # 18 p. 3337 - 3340
