2-硝基-N,N-二(4-硝基苯基)苯胺合成路线 (共 11 条)
反应条件
potassium carbonate in dimethyl sulfoxide T=125 - 130°C; 4.3 h;
参考文献
Gorvin, John H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1331 - 1336
反应条件
potassium carbonate in dimethyl sulfoxide T=125 - 130°C; 4 h;
参考文献
Gorvin, John H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1331 - 1336
反应条件
potassium tert-butylate in dimethyl sulfoxide T=125 - 130°C; 4 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1331 - 1336
反应条件
copper(II) nitrate in acetic anhydride T=20°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 47, # 44 p. 7667 - 7669
反应条件
1: 90 percent / Cs2CO3 / dimethylsulfoxide / 5 h / 145 - 150 °C 2: 74 percent / potassium t-butoxide / dimethylsulfoxide / 4 h / 125 - 130 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1331 - 1336
反应条件
1: 86 percent / Cs2CO3 / dimethylsulfoxide / 5.5 h / 140 °C 2: 76 percent / K2CO3 / dimethylsulfoxide / 4 h / 125 - 130 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1331 - 1336
反应条件
1: 90 percent / Na2CO3, copper bronze / pyridine / 4 h / Heating 2: 76 percent / K2CO3 / dimethylsulfoxide / 4 h / 125 - 130 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1331 - 1336
反应条件
1: 86 percent / Cs2CO3 / dimethylsulfoxide / 5.5 h / 140 °C 2: 76 percent / K2CO3 / dimethylsulfoxide / 4 h / 125 - 130 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1331 - 1336
反应条件
1: 66 percent / Cs2CO3 / dimethylsulfoxide / 5.5 h / 125 - 130 °C 2: 76 percent / K2CO3 / dimethylsulfoxide / 4 h / 125 - 130 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1331 - 1336
反应条件
1: 77 percent / potassium t-butoxyde / dimethylsulfoxide / 72 h / 20 - 25 °C 2: 74 percent / potassium t-butoxide / dimethylsulfoxide / 4 h / 125 - 130 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1331 - 1336