1,4-亚苯基二(二苯基膦)合成路线 （共 8 条）
反应条件
dichloro bis(acetonitrile) palladium(II) in benzene T=50°C; 53 h;
参考文献
Tunney, S. E.; Stille, J. K.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 748 - 753
反应条件
copper(l) iodide; caesium carbonate in toluene T=110°C; 24 h;
参考文献
Van Allen, Derek; Venkataraman
Journal of Organic Chemistry, 2003 , vol. 68, # 11 p. 4590 - 4593
反应条件
[NiCl2(PPh3)2]; potassium tert-butylate in 1,4-dioxane T=90°C; 10 h; Inert atmosphere;
参考文献
Sun, Meng; Zhang, Hong-Yu; Han, Qi; Yang, Kuo; Yang, Shang-Dong
Chemistry - A European Journal, 2011 , vol. 17, # 35 p. 9566 - 9570
反应条件
diethyl-acetamide; palladium diacetate T=70 - 80°C;
参考文献
Brauer, David J.; Hingst, Martin; Kottsieper, Konstantin W.; Liek, Christian; Nickel, Thomas; Tepper, Michael; Stelzer, Othmar; Sheldrick, William S.
Journal of Organometalic Chemistry, 2002 , vol. 645, # 1-2 p. 14 - 26
反应条件
in tetrahydrofuran; methanol 96 h; Inert atmosphereMolecular sieveReflux;
参考文献
Li, Jie; Lutz, Martin; Spek, Anthony L.; Van Klink, Gerard P.M.; Van Koten, Gerard; Klein Gebbink, Robertus J.M.
Journal of Organometallic Chemistry, 2010 , vol. 695, # 24 p. 2618 - 2628
反应条件
1: 1.) Li / 1.) THF, overnight, 2.) THF 2: 87 percent / (MeCN)2PdCl2 / benzene / 53 h / 50 °C View Scheme
参考文献
Tunney, S. E.; Stille, J. K.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 748 - 753
参考文献
Papp; Kovacs; Benyei; Laurenczy; Nadasdi; Joo
Canadian Journal of Chemistry, 2001 , vol. 79, # 5-6 p. 635 - 641
参考文献
Schindlbauer,H.; Hilzensauer,V.
Monatshefte fuer Chemie, 1967 , vol. 98, # 4 p. 1196 - 1200
