反应条件
1: With n-butyllithium; N,N,N',N'',N''-pentamethyldiethylenetriamine in tetrahydrofuran; hexane T=-74 - -70°C; 3.5 h; 2: With boric acid trimethyl ester; dihydrogen peroxide in tetrahydrofuran; hexane; acetic acid T=20°C;
参考文献
Eisai RandD Management Co., Ltd.; CLARK, Richard; MATSUURA, Fumiyoshi; SHINODA, Masanobu; HIROTA, Shinsuke; KIRA, Kazunobu; AZUMA, Hiroshi; TAKEMURA, Atsushi; YASUI, So; KUSANO, Kazutomi; MIKAMOTO, Masaki; OMAE, Takao
Patent: WO2011/145747 A1, 2011 ;
Location in patent: Page/Page column 97-98 ;
WO 2011/145747 A1
