反应条件
1: 51 percent / p-toluenesulfonic acid (pTSA), trimethyl orthoformate / 24 h / Heating
2: 6percent aq. NH4OH / methanol / 2 h / Heating
3: p-toluenesulfonic acid (pTSA) / dioxane; benzene / 48 h / Heating; azeotropic removal of water
4: 70 percent / dichlorodicyanobenzoquinone (DDQ) / dioxane / 10 h / Heating
View Scheme
参考文献
Hagen, Timothy J.; Narayanan, Krishnaswamy; Names, Jeffrey; Cook, James M.
Journal of Organic Chemistry, 1989 , vol. 54, # 9 p. 2170 - 2178