N,N-二乙基亚磷酰胺二叔丁酯合成路线 （共 13 条）
反应条件
triethylamine in diethyl ether T=20°C; 2 h;
参考文献
Australian Journal of Chemistry, , vol. 44, # 2 p. 233 - 252
反应条件
1: PCl3 / Heating 2: diethyl ether / 20 °C View Scheme
参考文献
Phosphorus, Sulfur and Silicon and Related Elements, , vol. 164, p. 277 - 291
反应条件
1: 63 percent / HCl / petroleum ether / Ambient temperature View Scheme
参考文献
Doklady Chemistry, , vol. 302, p. 299 - 302
Dokl. Akad. Nauk SSSR Ser. Khim., , vol. 302, # 6 p. 1380 - 1383
反应条件
in diethyl ether T=20°C;
参考文献
Phosphorus, Sulfur and Silicon and Related Elements, , vol. 164, p. 277 - 291
参考文献
Doklady Chemistry, , vol. 302, p. 299 - 302
Dokl. Akad. Nauk SSSR Ser. Khim., , vol. 302, # 6 p. 1380 - 1383
反应条件
1H-tetrazole; 3-chloro-benzenecarboperoxoic acid 1.) THF, 20 deg C, 15 min. 2.) THF, CH2Cl2, 20 deg C, 5 min; Yield given. Multistep reaction;
参考文献
Perich, John W.; Johns, R. B.
Synthesis, 1988 , # 2 p. 142 - 144
反应条件
1H-tetrazole; tert.-butylhydroperoxide in tetrahydrofuran
参考文献
Dore, Timothy M.; Zhu, Yue; Reddie, Khalilah G.; Lauderdale, James D.
Patent: US2010/48502 A1, 2010 ;
反应条件
1H-tetrazole; tert.-butylhydroperoxide; triethylamine in tetrahydrofuran; water; acetonitrile
参考文献
Dore, Timothy M.; Zhu, Yue; Reddie, Khalilah G.; Lauderdale, James D.
Patent: US2010/48502 A1, 2010 ;
反应条件
1H-tetrazole; 3-chloro-benzenecarboperoxoic acid
参考文献
Molecular Pharmacology, , vol. 62, # 5 p. 1249 - 1257
反应条件
1: With 1H-tetrazole in tetrahydrofuran
T=20°C; 0.333333 h;
2: With 3-chloro-benzenecarboperoxoic acid in tetrahydrofuran; dichloromethane
T=-70 - 20°C; 0.0833333 h;
参考文献
Arizona Broad of Regents acting for and on behalf of Arizona State University
Patent: US7018987 B1, 2006 ;
Location in patent: Page/Page column 10-11 ;
