反应条件
Multi-step reaction with 2 steps 1: SOCl2, collidine / tetrahydrofuran / 0.17 h / 0 °C2: 1.) DIBAL-H; 2.) Me2CO, iPrOH / 1.) 0 deg C; 2.) 20 deg C;
参考文献
Holland, Herbert L.; Rao, J. Appa; Chenchaiah, P. Chinna Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2027 - 2032