2-[[[4-(3-甲氧基丙氧基)-3-甲基吡啶-2-基]甲基]硫代]-1H-苯并咪唑合成路线 (共 17 条)
反应条件
3-chloro-benzenecarboperoxoic acid in methanol; chloroform T=-25 - -20°C;
参考文献
Reddy, Ganta Madhusudhan; Mukkanti, Kaga; Bhaskar, Boluggodu Vijaya; Reddy, Padi Pratap
Synthetic Communications, 2009 , vol. 39, # 2 p. 278 - 290
反应条件
peracetic acid; sodium carbonate in dichloromethane T=20°C; 20 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 43, # 6 p. 1447 - 1453
反应条件
sodium hydroxide; dihydrogen peroxide; sodium tungstate in methanol; water T=20°C; 0.666667 h; Product distribution / selectivity;
参考文献
US2009/5570 A1, ;
Page/Page column 3-4 ;
反应条件
sodium hydroxide; N-chloro-succinimide; water in acetonitrile T=0 - 5°C; 2 h; Product distribution / selectivity;
参考文献
WO2006/24890 A1, ;
Page/Page column 6-7 ;
反应条件
N-ethyl-N,N-diisopropylamine; isopropylbenzene hydroperoxide; titanium(IV) isopropylate in water; toluene
参考文献
US5948789 A1, ;
US 5948789 A
反应条件
N-ethyl-N,N-diisopropylamine; isopropylbenzene hydroperoxide; titanium(IV) isopropylate in water; toluene
参考文献
US5948789 A1, ;
US 5948789 A
反应条件
1: in sodium hydroxide; diethyl ether; dichloromethane T=-10°C; 1.08333 h; 2: With triethylamine in diethyl ether; dichloromethane T=0 - 20°C;
参考文献
EP1818331 A1, ;
Page/Page column 6 ;