反应条件
1: 1.) hexamethyldisilazane, chlorotrimethylsilane; 2.) hexamethyldisilazane, CF3SO3SiMe3, NH3 / 1.) reflux, 16 h; 2.) 150 deg C, 3 d (sealed bomb) 2: 47 percent / SnCl2*2H2O / dimethylformamide; 1,2-dimethoxy-ethane / 50 °C 3: 92 percent / adenosine deaminase / dimethylsulfoxide; H2O / 72 h / Ambient temperature; 0.1M sodium phosphate buffer View Scheme
参考文献
Robins, Morris J.; Hansske, Fritz; Bernier, Salwa E.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 3360 - 3364
