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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
鸟苷
合成路线
（共 235 条）
118-00-3
鸟苷
→
反应条件
86-01-1
鸟苷三磷酸
反应条件
human deoxycytidine kinase; adenosine 5'-triphosphoric acid; magnesium chloride in water T=37°C; phosphorylation; pH=7.5; Enzyme kinetics;
参考文献
Nucleosides and Nucleotides, , vol. 18, # 4-5 p. 857 - 860
118-00-3
鸟苷
→
反应条件
104227-86-3
2-[2-(2-氨基-9h-嘌呤-9-基)乙基]-1,3-丙二醇
反应条件
1.1: dimethylsulfoxide / 24 h / 20 °C 1.2: 85 percent / aq. HCl / dimethylsulfoxide / 2 h / 70 °C 2.1: 93 percent / 1-methyl-pyrrolidin-2-one / 1 h / 150 °C 3.1: 1-methyl-pyrrolidin-2-one / 2 h / 120 °C 4.1: HCOONH4 / Pd/C / methanol / 4 h / Heating 5.1: aq. NaOH / 0.5 h / Heating 6.1: 83 percent / 1-methyl-pyrrolidin-2-one / 5 h / 150 °C 7.1: 99 percent / Et3N; DMAP / CH2Cl2 / 2.5 h / 20 °C 8.1: 60 percent / H2; Et3N / Pd/C / ethanol / 8 h / 80 - 85 °C / 2250.18 Torr 9.1: 99 percent / aq. MeNH2 / 0.25 h / 20 °C View Scheme
参考文献
Synthesis, , # 12 p. 2026 - 2034
118-00-3
鸟苷
→
反应条件
104227-87-4
泛昔洛韦
反应条件
1.1: dimethylsulfoxide / 24 h / 20 °C 1.2: 85 percent / aq. HCl / dimethylsulfoxide / 2 h / 70 °C 2.1: 93 percent / 1-methyl-pyrrolidin-2-one / 1 h / 150 °C 3.1: 1-methyl-pyrrolidin-2-one / 2 h / 120 °C 4.1: HCOONH4 / Pd/C / methanol / 4 h / Heating 5.1: aq. NaOH / 0.5 h / Heating 6.1: 83 percent / 1-methyl-pyrrolidin-2-one / 5 h / 150 °C 7.1: 99 percent / Et3N; DMAP / CH2Cl2 / 2.5 h / 20 °C 8.1: 60 percent / H2; Et3N / Pd/C / ethanol / 8 h / 80 - 85 °C / 2250.18 Torr 9.1: 99 percent / aq. MeNH2 / 0.25 h / 20 °C 10.1: 97 percent / pyridine; DMAP / tetrahydrofuran / 3 h / 20 °C View Scheme
参考文献
Synthesis, , # 12 p. 2026 - 2034
118-00-3
鸟苷
→
反应条件
146-77-0
2-氯腺嘌呤核苷
反应条件
1: pyridine / dimethylformamide / 4.5 h / 75 °C 2: 70.85 percent / Et4NCl, Me2NPh, POCl3 / acetonitrile / 0.17 h / Heating 3: Ph3CCl, K2CO3, isoamyl nitrite / CH2Cl2 / 0.5 h / Heating 4: conc. NH4OH / tetrahydrofuran / 72 h / Ambient temperature View Scheme
参考文献
El-Tayeb, Ali; Gollos, Sabrina
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 2 p. 436 - 447
118-00-3
鸟苷
→
反应条件
80394-72-5
5-氨基-3-beta-D-呋喃核糖基咪唑并(4,5-d)(1,3)恶嗪-7(3H)-酮
+
13276-43-2
2-氯肌苷
+
146-80-5
黄嘌呤核苷
反应条件
sodium acetate; sodium chloride; sodium nitrite in water T=37°C; pH=3.2; 2 h; Product distribution;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 11, # 21 p. 2937 - 2941
64656-29-7
+
118-00-3
鸟苷
→
反应条件
132628-16-1
反应条件
Yield given. Multistep reaction;
参考文献
Rao, M. Vaman; Reese, Colin B.; Schehlmann, Volker; Yu, Pak Sang
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 1 p. 43 - 56
118-00-3
鸟苷
→
反应条件
146-80-5
黄嘌呤核苷
反应条件
oxygen; nitrogen(II) oxide in dimethyl sulfoxide 1 h; Ambient temperature;
参考文献
Nagano, Tetsuo; Takizawa, Hiromasa; Hirobe, Masaaki
Tetrahedron Letters, 1995 , vol. 36, # 45 p. 8239 - 8242
118-00-3
鸟苷
→
反应条件
80394-72-5
5-氨基-3-beta-D-呋喃核糖基咪唑并(4,5-d)(1,3)恶嗪-7(3H)-酮
+
13276-43-2
2-氯肌苷
+
146-80-5
黄嘌呤核苷
反应条件
sodium acetate; sodium chloride; sodium nitrite in water T=37°C; pH=3.2; 2 h; Product distribution;
参考文献
Suzuki, Toshinori; Ide, Hiroshi; Yamada, Masaki; Morii, Takashi; Makino, Keisuke
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 21 p. 2937 - 2941
18412-81-2
+
118-00-3
鸟苷
→
反应条件
1187-84-4
+
2140-65-0
反应条件
potassium hydroxide in water T=65°C; 12 h; pH = 10.5;
参考文献
Yamauchi, Kiyoshi; Hisanaga, Yorisato; Kinoshita, Masayoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1941 - 1942
118-00-3
鸟苷
→
反应条件
2004-07-1
反应条件
1: 4-dimethylaminopyridine; triethylamine 2: phosphorus oxychloride; tetraethylammonium chloride; N,N-dimethylaniline / acetonitrile 3: NH3 / methanol View Scheme
参考文献
Volpini, Rosaria; Marucci, Gabriella; Buccioni, Michela; DalBen, Diego; Lambertucci, Catia; Lammi, Carmen; Mishra, Ram C.; Thomas, Ajiroghene; Cristalli, Gloria
ChemMedChem, 2011 , vol. 6, # 6 p. 1074 - 1080
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