1,3,3-三甲基-2-亚甲基吲哚啉合成路线 （共 94 条）
反应条件
1: sodium isothiocyanate With benzoyl chloride in acetone
Reflux;
2: 1,3-dihydro-1,3,3-trimethyl-2-methyleneindoline in acetone
T=20°C; Reflux;
3: With sodium methylate in methanol
Reflux;
参考文献
Shank, Nathaniel I.; Zanotti, Kimberly J.; Lanni, Frederick; Berget, Peter B.; Armitage, Bruce A.
Journal of the American Chemical Society, 2009 , vol. 131, # 36 p. 12960 - 12969
反应条件
carbon dioxide; sodium nitrite in water
T=35 - 40°C; P=37503 Torr; 3 h;
参考文献
Raue, Roderich; Brack, Alfred; Lange, Karl H.
Angewandte Chemie, 1991 , vol. 103, # 12 p. 1689 - 1690
参考文献
Keum, Sam-Rok; Lee, Ki-Bong; Kazmaier, Peter M.; Manderville, Richard A.; Buncel, Erwin
Magnetic Resonance in Chemistry, 1992 , vol. 30, # 11 p. 1128 - 1131
反应条件
acetic anhydride
T=50°C; 3 h;
参考文献
KODAK POLYCHROME GRAPHICS GMBH
Patent: WO2004/52995 A1, 2004 ;
Location in patent: Page 24 ;
