1,3,3-三甲基-2-亚甲基吲哚啉合成路线 (共 94 条)
反应条件
trimethyl-oxonium tetrafluoroborate; phosphorus tribromide 1) dichloromethan, reflux, 2 h, 2) chloroform 25 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Gamon, Norbert; Reichardt, Christian
Liebigs Annalen der Chemie, 1980 , # 12 p. 2072 - 2094
反应条件
phosphorus tribromide 1) dichloromethan, reflux, 2 h, 2) benzene, ether, 0 deg C, 30 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Gamon, Norbert; Reichardt, Christian
Liebigs Annalen der Chemie, 1980 , # 12 p. 2072 - 2094
反应条件
in ethanol 0.25 h; Irradiation;
参考文献
Torres; Vazquez; Gonzalez
Synthetic Communications, 1995 , vol. 25, # 1 p. 105 - 110
参考文献
Balny,C. et al.
Tetrahedron Letters, 1968 , p. 5097 - 5099
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Berman et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 5605,5607, 5608
反应条件
in ethanol 0.25 h; Irradiation;
参考文献
Torres; Vazquez; Gonzalez
Synthetic Communications, 1995 , vol. 25, # 1 p. 105 - 110
参考文献
Keum, Sam-Rok; Lee, Ki-Bong; Kazmaier, Peter M.; Manderville, Richard A.; Buncel, Erwin
Magnetic Resonance in Chemistry, 1992 , vol. 30, # 11 p. 1128 - 1131
参考文献
Lauerer et al.
Zeitschrift fuer Physikalische Chemie (Muenchen, Germany), 1957 , vol. 10, p. 236,242,256
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Coenen
Angewandte Chemie, 1949 , vol. 61, p. 11,14
参考文献
Coenen
Chemische Berichte, 1949 , vol. 82, p. 66,69
参考文献
Lauerer et al.
Zeitschrift fuer Physikalische Chemie (Muenchen, Germany), vol. 10, p. 1957 236, 262
反应条件
1,2-dichloro-benzene; trichlorophosphate anschliessendes Hydrolysieren;
参考文献
I.G.Farbenind.
Patent: DE677207 , 1937 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 25, p. 171