N-羟甲基邻苯二甲酰亚胺合成路线 （共 74 条）
反应条件
18-crown-6 ether; methanesulphonyl fluoride; cesium fluoride in tetrahydrofuran
参考文献
Makio, K.; Yoshioka, H.
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 677 - 684
反应条件
1.1: thionyl chloride / 4 h / 75 °C / Inert atmosphere 2.1: sodium iodide / acetone / 4 h / 20 °C / Darkness 3.1: diethylzinc / hexane; dichloromethane / 18 h / 20 °C / Inert atmosphere 3.2: 4 h / Inert atmosphere View Scheme
参考文献
Maury, Julien; Mouysset, Dominique; Feray, Laurence; Marque, Sylvain R. A.; Siri, Didier; Bertrand, Michele P.
Chemistry - A European Journal, 2012 , vol. 18, # 11 p. 3241 - 3247
反应条件
18-crown-6 ether; methanesulphonyl fluoride; cesium fluoride in tetrahydrofuran
参考文献
Makio, K.; Yoshioka, H.
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 677 - 684
反应条件
sulfuric acid; 4-methylaminonitrobenzene T=50°C; 3 h;
参考文献
Wilshire, John F. K.
Australian Journal of Chemistry, 1990 , vol. 43, # 11 p. 1817 - 1826
参考文献
Vinkler; Szabo
Acta Chimica Academiae Scientiarum Hungaricae, 1951 , vol. 1, p. 103,106
Chem.Abstr., 1952 , p. 2500
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Buc
Journal of the American Chemical Society, 1947 , vol. 69, p. 254
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Hellmann et al.
Justus Liebigs Annalen der Chemie, 1959 , vol. 626, p. 35,45
反应条件
1: concentrated sulfuric acid 2: 170 °C View Scheme
参考文献
Buc
Journal of the American Chemical Society, 1947 , vol. 69, p. 254
参考文献
Buc
Journal of the American Chemical Society, 1947 , vol. 69, p. 254
参考文献
Buc
Journal of the American Chemical Society, 1947 , vol. 69, p. 254
反应条件
thionyl chloride in dichloromethane; N,N-dimethyl-formamide T=20°C; 2.5 h;
参考文献
Huang, Zhongyan; Xu, Jiaxi
Tetrahedron, 2013 , vol. 69, # 3 p. 1050 - 1056
参考文献
Sachs
Chemische Berichte, 1898 , vol. 31, p. 1229
